1-[[(2,3,5,6-tetrachloro-4-hydroxyphenoxy)acetyl]oxy]-2,5-pyrrolidinedione

Base Information

Chemical Name:1-[[(2,3,5,6-tetrachloro-4-hydroxyphenoxy)acetyl]oxy]-2,5-pyrrolidinedione
CAS No.:329785-19-5
Molecular Formula:C₁₂H₇Cl₄NO₆
Molecular Weight:403.003
Hs Code.:

Synonyms:1-[[(2,3,5,6-tetrachloro-4-hydroxyphenoxy)acetyl]oxy]-2,5-pyrrolidinedione

Suppliers and Price of 1-[[(2,3,5,6-tetrachloro-4-hydroxyphenoxy)acetyl]oxy]-2,5-pyrrolidinedione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[[(2,3,5,6-tetrachloro-4-hydroxyphenoxy)acetyl]oxy]-2,5-pyrrolidinedione

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Technology Process of 1-[[(2,3,5,6-tetrachloro-4-hydroxyphenoxy)acetyl]oxy]-2,5-pyrrolidinedione

There total 2 articles about 1-[[(2,3,5,6-tetrachloro-4-hydroxyphenoxy)acetyl]oxy]-2,5-pyrrolidinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.3%

: 6066-82-6
1-hydroxy-pyrrolidine-2,5-dione

: 951-11-1
(2,3,5,6-tetrachloro-4-hydroxyphenoxy)acetic acid

: 329785-19-5
1-[[(2,3,5,6-tetrachloro-4-hydroxyphenoxy)acetyl]oxy]-2,5-pyrrolidinedione

Guidance literature:: With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In N,N-dimethyl-formamide; at 20 ℃; for 24h;
DOI:10.1021/jf0010578

Reference yield:

: 87-87-6
2,3,5,6-tetrachlorobenzene-1,4-diol

: 329785-19-5
1-[[(2,3,5,6-tetrachloro-4-hydroxyphenoxy)acetyl]oxy]-2,5-pyrrolidinedione

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / aq. NaOH / 4 h / 80 °C

2: 19.3 percent / EDC / dimethylformamide / 24 h / 20 °C

With sodium hydroxide; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In N,N-dimethyl-formamide;
DOI:10.1021/jf0010578