13-Aza-3-methoxy-7-methyl-18-nor-5,6-seco-Δ^9,11-estrone

Base Information

Chemical Name:13-Aza-3-methoxy-7-methyl-18-nor-5,6-seco-Δ^9,11-estrone
CAS No.:82938-28-1
Molecular Formula:C₁₈H₂₃NO₂
Molecular Weight:285.386
Hs Code.:

13-Aza-3-methoxy-7-methyl-18-nor-5,6-seco-Δ<sup>9,11</sup>-estrone

Synonyms:13-Aza-3-methoxy-7-methyl-18-nor-5,6-seco-Δ^9,11-estrone

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Chemical Property of 13-Aza-3-methoxy-7-methyl-18-nor-5,6-seco-Δ^9,11-estrone

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Technology Process of 13-Aza-3-methoxy-7-methyl-18-nor-5,6-seco-Δ^9,11-estrone

There total 4 articles about 13-Aza-3-methoxy-7-methyl-18-nor-5,6-seco-Δ^9,11-estrone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82938-20-3
3-methyl-1-(4-methoxyphenyl)-1-butanone

: 82938-28-1
13-Aza-3-methoxy-7-methyl-18-nor-5,6-seco-Δ^9,11-estrone

Guidance literature:: Multi-step reaction with 5 steps

1: 1) NaH / 1) THF, <5 degC, 2) 60 degC, 6h

2: 80 percent / LAH / diethyl ether / 3 h / 0 °C

3: 34 percent / 4 h / 190 - 200 °C

4: 54 percent / NaBH₄ / aq. ethanol / 0 °C / 1) addition of 2N HCl in 10min intervalls over 5h 2) pH 3, 1h

5: 35 percent / PTS / benzene / 0.75 h / Heating

With sodium tetrahydroborate; lithium aluminium tetrahydride; pyridinium p-toluenesulfonate; sodium hydride; In diethyl ether; ethanol; benzene;

Reference yield:

: 82938-23-6,82938-24-7
1-amino-3-(p-methoxyphenyl)-5-methyl-hex-2-ene

: 82938-28-1
13-Aza-3-methoxy-7-methyl-18-nor-5,6-seco-Δ^9,11-estrone

Guidance literature:: Multi-step reaction with 3 steps

1: 34 percent / 4 h / 190 - 200 °C

2: 54 percent / NaBH₄ / aq. ethanol / 0 °C / 1) addition of 2N HCl in 10min intervalls over 5h 2) pH 3, 1h

3: 35 percent / PTS / benzene / 0.75 h / Heating

With sodium tetrahydroborate; pyridinium p-toluenesulfonate; In ethanol; benzene;

Reference yield:

: 82938-21-4,82938-22-5
Cyano-2-(p-methoxyphenyl)-4-methyl-pent-1-ene

: 82938-28-1
13-Aza-3-methoxy-7-methyl-18-nor-5,6-seco-Δ^9,11-estrone

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / LAH / diethyl ether / 3 h / 0 °C

2: 34 percent / 4 h / 190 - 200 °C

3: 54 percent / NaBH₄ / aq. ethanol / 0 °C / 1) addition of 2N HCl in 10min intervalls over 5h 2) pH 3, 1h

4: 35 percent / PTS / benzene / 0.75 h / Heating

With sodium tetrahydroborate; lithium aluminium tetrahydride; pyridinium p-toluenesulfonate; In diethyl ether; ethanol; benzene;