4-chloro-benzenesulfonic acid 2-(3-furan-2-yl-propionyl)-4,6-diiodophenyl ester

Base Information

Chemical Name:4-chloro-benzenesulfonic acid 2-(3-furan-2-yl-propionyl)-4,6-diiodophenyl ester
CAS No.:784210-44-2
Molecular Formula:C₁₉H₁₃ClI₂O₅S
Molecular Weight:642.637
Hs Code.:

Synonyms:4-chloro-benzenesulfonic acid 2-(3-furan-2-yl-propionyl)-4,6-diiodophenyl ester

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Chemical Property of 4-chloro-benzenesulfonic acid 2-(3-furan-2-yl-propionyl)-4,6-diiodophenyl ester

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Technology Process of 4-chloro-benzenesulfonic acid 2-(3-furan-2-yl-propionyl)-4,6-diiodophenyl ester

There total 3 articles about 4-chloro-benzenesulfonic acid 2-(3-furan-2-yl-propionyl)-4,6-diiodophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 784210-32-8
4-chloro-benzenesulfonic acid 2,4,6-triiodophenyl ester

: 54536-91-3
3-(2-furyl)-propanoic acid chloride

: 784210-44-2
4-chloro-benzenesulfonic acid 2-(3-furan-2-yl-propionyl)-4,6-diiodophenyl ester

Guidance literature:: 4-chloro-benzenesulfonic acid 2,4,6-triiodophenyl ester; With isopropylmagnesium chloride; In tetrahydrofuran; at -78 ℃; for 0.5h;

3-(2-furyl)-propanoic acid chloride; In tetrahydrofuran; at -78 - 20 ℃;
DOI:10.1002/anie.200460417

Reference yield:

: 609-23-4,72100-00-6
2,4,6-Triiodophenol

: 784210-44-2
4-chloro-benzenesulfonic acid 2-(3-furan-2-yl-propionyl)-4,6-diiodophenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 90 percent / pyridine / 20 °C

2.1: iPrMgCl / tetrahydrofuran / 0.5 h / -78 °C

2.2: 65 percent / CuCN*2LiCl / tetrahydrofuran / -78 - 20 °C

With pyridine; isopropylmagnesium chloride; In tetrahydrofuran;
DOI:10.1002/anie.200460417

Reference yield:

: 98-60-2
4-chlorobenzenesulfonyl chloride

: 784210-44-2
4-chloro-benzenesulfonic acid 2-(3-furan-2-yl-propionyl)-4,6-diiodophenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 90 percent / pyridine / 20 °C

2.1: iPrMgCl / tetrahydrofuran / 0.5 h / -78 °C

2.2: 65 percent / CuCN*2LiCl / tetrahydrofuran / -78 - 20 °C

With pyridine; isopropylmagnesium chloride; In tetrahydrofuran;
DOI:10.1002/anie.200460417