methyl m-xylenethiocarboxylate

Base Information

• Chemical Name: methyl m-xylenethiocarboxylate
• CAS No.: 39248-75-4
• Molecular Formula: C₁₀H₁₂OS
• Molecular Weight: 180.271

Synonyms:methyl m-xylenethiocarboxylate

Chemical Property of methyl m-xylenethiocarboxylate

Chemical Property:

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Technology Process of methyl m-xylenethiocarboxylate

There total 2 articles about methyl m-xylenethiocarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

C2H3OS(1+)*F6Sb(1-) (75626-81-2) + m-xylene (108-38-3,104809-90-7) → methyl m-xylenethiocarboxylate (39248-75-4)

Guidance literature:

In liquid sulphur dioxide; at -70 ℃; for 0.166667h;

DOI:10.1021/jo00315a040

Reference yield:

m-xylene (108-38-3,104809-90-7) + methyl thiochloroformate (18369-83-0) → methyl m-xylenethiocarboxylate (39248-75-4)

Guidance literature:

With aluminium trichloride;

Reference yield: 78.0%

methyl m-xylenethiocarboxylate (39248-75-4) → 2,4-dimethyl-benzoic acid (611-01-8)

Guidance literature:

With sodium hydroxide; for 1h;

DOI:10.1021/jo00315a040

upstream raw materials:

m-xylene

methyl thiochloroformate

C₂H₃OS⁽¹⁺⁾*F₆Sb^(1-)

Downstream raw materials:

2,4-dimethyl-benzoic acid

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