2-(5-(4-t-butylphenyl)-1,3,4-oxadiazole-2-yl)-5-(5-(3-(4-(2-(2-hydroxyphenyl)-4,5-diphenyl-1H-imidazole-1-yl)phenoxy)phenyl)-1,3,4-oxadiazole-2-yl)benzene-1,4-diol

Base Information

Chemical Name:2-(5-(4-t-butylphenyl)-1,3,4-oxadiazole-2-yl)-5-(5-(3-(4-(2-(2-hydroxyphenyl)-4,5-diphenyl-1H-imidazole-1-yl)phenoxy)phenyl)-1,3,4-oxadiazole-2-yl)benzene-1,4-diol
CAS No.:1253119-91-3
Molecular Formula:C₅₃H₄₀N₆O₆
Molecular Weight:856.937
Hs Code.:

2-(5-(4-t-butylphenyl)-1,3,4-oxadiazole-2-yl)-5-(5-(3-(4-(2-(2-hydroxyphenyl)-4,5-diphenyl-1H-imidazole-1-yl)phenoxy)phenyl)-1,3,4-oxadiazole-2-yl)benzene-1,4-diol

Synonyms:2-(5-(4-t-butylphenyl)-1,3,4-oxadiazole-2-yl)-5-(5-(3-(4-(2-(2-hydroxyphenyl)-4,5-diphenyl-1H-imidazole-1-yl)phenoxy)phenyl)-1,3,4-oxadiazole-2-yl)benzene-1,4-diol

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Chemical Property of 2-(5-(4-t-butylphenyl)-1,3,4-oxadiazole-2-yl)-5-(5-(3-(4-(2-(2-hydroxyphenyl)-4,5-diphenyl-1H-imidazole-1-yl)phenoxy)phenyl)-1,3,4-oxadiazole-2-yl)benzene-1,4-diol

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Technology Process of 2-(5-(4-t-butylphenyl)-1,3,4-oxadiazole-2-yl)-5-(5-(3-(4-(2-(2-hydroxyphenyl)-4,5-diphenyl-1H-imidazole-1-yl)phenoxy)phenyl)-1,3,4-oxadiazole-2-yl)benzene-1,4-diol

There total 15 articles about 2-(5-(4-t-butylphenyl)-1,3,4-oxadiazole-2-yl)-5-(5-(3-(4-(2-(2-hydroxyphenyl)-4,5-diphenyl-1H-imidazole-1-yl)phenoxy)phenyl)-1,3,4-oxadiazole-2-yl)benzene-1,4-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 1253119-90-2
2-(5-(3-(4-aminophenoxy)phenyl)-1,3,4-oxadiazole-2-yl)-5-(5-(4-t-butylphenyl)-1,3,4-oxadiazole-2-yl)benzene-1,4-diol

: 100-52-7
benzaldehyde

: 90-02-8
salicylaldehyde

: 1253119-91-3
2-(5-(4-t-butylphenyl)-1,3,4-oxadiazole-2-yl)-5-(5-(3-(4-(2-(2-hydroxyphenyl)-4,5-diphenyl-1H-imidazole-1-yl)phenoxy)phenyl)-1,3,4-oxadiazole-2-yl)benzene-1,4-diol

Guidance literature:: With ammonium acetate; acetic acid; at 20 - 110 ℃; for 12h;

Reference yield:

: 350-46-9,178603-76-4
4-Fluoronitrobenzene

: 1253119-91-3
2-(5-(4-t-butylphenyl)-1,3,4-oxadiazole-2-yl)-5-(5-(3-(4-(2-(2-hydroxyphenyl)-4,5-diphenyl-1H-imidazole-1-yl)phenoxy)phenyl)-1,3,4-oxadiazole-2-yl)benzene-1,4-diol

Guidance literature:: Multi-step reaction with 8 steps

1: potassium carbonate / dimethyl sulfoxide / 12 h / 130 °C

2: hydrogenchloride / water / 12 h / 110 °C

3: hydrazine hydrate / ethanol / 24 h / Reflux

4: tetrahydrofuran / 12 h / 20 °C

5: trichlorophosphate / 12 h / 90 °C

6: boron tribromide / dichloromethane / -78 - 0 °C

7: hydrogen / 5%-palladium/activated carbon / tetrahydrofuran / 18 h

8: ammonium acetate; acetic acid / 12 h / 20 - 110 °C

With hydrogenchloride; ammonium acetate; hydrogen; boron tribromide; potassium carbonate; hydrazine hydrate; acetic acid; trichlorophosphate; 5%-palladium/activated carbon; In tetrahydrofuran; ethanol; dichloromethane; water; dimethyl sulfoxide;

Reference yield:

: 149697-46-1
2,5-bis(hexyloxy)terephthalic acid diethyl ester

: 1253119-91-3
2-(5-(4-t-butylphenyl)-1,3,4-oxadiazole-2-yl)-5-(5-(3-(4-(2-(2-hydroxyphenyl)-4,5-diphenyl-1H-imidazole-1-yl)phenoxy)phenyl)-1,3,4-oxadiazole-2-yl)benzene-1,4-diol

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium hydroxide / ethanol / 12 h / Reflux

1.2: pH 4

2.1: N,N-dimethyl-formamide; thionyl chloride / 6 h / 80 °C

3.1: tetrahydrofuran / 12 h / 20 °C

4.1: trichlorophosphate / 12 h / 90 °C

5.1: boron tribromide / dichloromethane / -78 - 0 °C

6.1: hydrogen / 5%-palladium/activated carbon / tetrahydrofuran / 18 h

7.1: ammonium acetate; acetic acid / 12 h / 20 - 110 °C

With thionyl chloride; ammonium acetate; hydrogen; boron tribromide; acetic acid; N,N-dimethyl-formamide; potassium hydroxide; trichlorophosphate; 5%-palladium/activated carbon; In tetrahydrofuran; ethanol; dichloromethane;