6-O-benzyl-5-deoxy-1,2-O-isopropylidene-3-trifluoromethylsulphonyl-α-D-xylo-hexofuranose

Base Information

Chemical Name:6-O-benzyl-5-deoxy-1,2-O-isopropylidene-3-trifluoromethylsulphonyl-α-D-xylo-hexofuranose
CAS No.:94530-15-1
Molecular Formula:C₁₇H₂₁F₃O₇S
Molecular Weight:426.411
Hs Code.:

Synonyms:6-O-benzyl-5-deoxy-1,2-O-isopropylidene-3-trifluoromethylsulphonyl-α-D-xylo-hexofuranose

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Chemical Property of 6-O-benzyl-5-deoxy-1,2-O-isopropylidene-3-trifluoromethylsulphonyl-α-D-xylo-hexofuranose

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Technology Process of 6-O-benzyl-5-deoxy-1,2-O-isopropylidene-3-trifluoromethylsulphonyl-α-D-xylo-hexofuranose

There total 5 articles about 6-O-benzyl-5-deoxy-1,2-O-isopropylidene-3-trifluoromethylsulphonyl-α-D-xylo-hexofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 94530-14-0
6-O-benzyl-5-deoxy-1,2-O-isopropylidene-α-D-xylo-hexofuranose

: 94530-15-1
6-O-benzyl-5-deoxy-1,2-O-isopropylidene-3-trifluoromethylsulphonyl-α-D-xylo-hexofuranose

Guidance literature:: With pyridine; In chloroform; at -10 ℃; for 1h;

Reference yield:

: 100-39-0
benzyl bromide

: 94530-15-1
6-O-benzyl-5-deoxy-1,2-O-isopropylidene-3-trifluoromethylsulphonyl-α-D-xylo-hexofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: 1) NaH (55percent dispersion in oil) / 1) DMF, 0 deg C, 2) r.t., overnight

2: TFA / methanol; CHCl₃ / 1 h / Ambient temperature

3: 98 percent / pyridine / CHCl₃ / 1 h / -10 °C

With pyridine; sodium hydride; trifluoroacetic acid; In methanol; chloroform;

Reference yield:

: 74152-55-9
5-deoxy-1,2-O-isopropylidene-3-(1-methoxy-1-methyl ethyl)-α-D-xylo-hexofuranose

: 94530-15-1
6-O-benzyl-5-deoxy-1,2-O-isopropylidene-3-trifluoromethylsulphonyl-α-D-xylo-hexofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: 1) NaH (55percent dispersion in oil) / 1) DMF, 0 deg C, 2) r.t., overnight

2: TFA / methanol; CHCl₃ / 1 h / Ambient temperature

3: 98 percent / pyridine / CHCl₃ / 1 h / -10 °C

With pyridine; sodium hydride; trifluoroacetic acid; In methanol; chloroform;