8-<4-<<<<<2-<(4-hydroxybenzylidene)ammonio>ethyl>amino>carbonyl>methyl>oxy>phenyl>-1,3-dipropylxanthine acetate

Base Information

Chemical Name:8-<4-<<<<<2-<(4-hydroxybenzylidene)ammonio>ethyl>amino>carbonyl>methyl>oxy>phenyl>-1,3-dipropylxanthine acetate
CAS No.:96896-81-0
Molecular Formula:C₂H₄O₂*C₂₈H₃₂N₆O₅
Molecular Weight:592.652
Hs Code.:

Synonyms:8-<4-<<<<<2-<(4-hydroxybenzylidene)ammonio>ethyl>amino>carbonyl>methyl>oxy>phenyl>-1,3-dipropylxanthine acetate

Suppliers and Price of 8-<4-<<<<<2-<(4-hydroxybenzylidene)ammonio>ethyl>amino>carbonyl>methyl>oxy>phenyl>-1,3-dipropylxanthine acetate

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Chemical Property of 8-<4-<<<<<2-<(4-hydroxybenzylidene)ammonio>ethyl>amino>carbonyl>methyl>oxy>phenyl>-1,3-dipropylxanthine acetate

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Technology Process of 8-<4-<<<<<2-<(4-hydroxybenzylidene)ammonio>ethyl>amino>carbonyl>methyl>oxy>phenyl>-1,3-dipropylxanthine acetate

There total 6 articles about 8-<4-<<<<<2-<(4-hydroxybenzylidene)ammonio>ethyl>amino>carbonyl>methyl>oxy>phenyl>-1,3-dipropylxanthine acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 64-19-7,77671-22-8
acetic acid

: 96865-92-8
8-<4-<<<<(2-aminoethyl)amino>carbonyl>methyl>oxy>phenyl>-1,3-dipropylxanthine

: 96896-81-0
8-<4-<<<<<2-<(4-hydroxybenzylidene)ammonio>ethyl>amino>carbonyl>methyl>oxy>phenyl>-1,3-dipropylxanthine acetate

Guidance literature:: In ethanol; for 2h; Heating;
DOI:10.1021/jm00147a038

Reference yield:

: 81250-34-2
1,3-dipropyl-5,6-diaminouracil

: 96896-81-0
8-<4-<<<<<2-<(4-hydroxybenzylidene)ammonio>ethyl>amino>carbonyl>methyl>oxy>phenyl>-1,3-dipropylxanthine acetate

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / acetic acid / methanol / 0.25 h / Heating

2: 71 percent / ferric chloride / 24 h / Heating

3: 99 percent / dimethylformamide

4: 75 percent / ethanol / 2 h / Heating

With iron(III) chloride; acetic acid; In methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00147a038

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 96896-81-0
8-<4-<<<<<2-<(4-hydroxybenzylidene)ammonio>ethyl>amino>carbonyl>methyl>oxy>phenyl>-1,3-dipropylxanthine acetate

Guidance literature:: Multi-step reaction with 5 steps

1: 60 percent / potassium carbonate / dimethylformamide / 72 h / 60 °C

2: 86 percent / acetic acid / methanol / 0.25 h / Heating

3: 71 percent / ferric chloride / 24 h / Heating

4: 99 percent / dimethylformamide

5: 75 percent / ethanol / 2 h / Heating

With iron(III) chloride; potassium carbonate; acetic acid; In methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00147a038