1,2-Dimethoxy-4-[4-(phenylmethoxy)-1-cyclohexen-1-yl]benzene

Base Information

Chemical Name:1,2-Dimethoxy-4-[4-(phenylmethoxy)-1-cyclohexen-1-yl]benzene
CAS No.:82732-16-9
Molecular Formula:C₂₁H₂₄O₃
Molecular Weight:324.42
Hs Code.:
DSSTox Substance ID:DTXSID301184117

Synonyms:DTXSID301184117;1,2-Dimethoxy-4-[4-(phenylmethoxy)-1-cyclohexen-1-yl]benzene;82732-16-9

Suppliers and Price of 1,2-Dimethoxy-4-[4-(phenylmethoxy)-1-cyclohexen-1-yl]benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-Dimethoxy-4-[4-(phenylmethoxy)-1-cyclohexen-1-yl]benzene

Chemical Property:

XLogP3:4.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:6
Exact Mass:324.17254462
Heavy Atom Count:24
Complexity:400

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)C2=CCC(CC2)OCC3=CC=CC=C3)OC

Technology Process of 1,2-Dimethoxy-4-[4-(phenylmethoxy)-1-cyclohexen-1-yl]benzene

There total 6 articles about 1,2-Dimethoxy-4-[4-(phenylmethoxy)-1-cyclohexen-1-yl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-Benzyloxy-1-(3,4-dimethoxy-phenyl)-cyclohexanol

: 82732-16-9
4-(benzyloxy)-1-(3,4-dimethoxyphenyl)cyclohex-1-ene

Guidance literature:: With toluene-4-sulfonic acid; In acetone; for 48h; Yield given; Ambient temperature;
DOI:10.1021/jo00141a015

Reference yield:

: 22428-87-1
4,4-ethylenedioxycyclohexan-1-ol

: 82732-16-9
4-(benzyloxy)-1-(3,4-dimethoxyphenyl)cyclohex-1-ene

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) KH / 1.) THF, 2.) 0 deg C, 30 min

2: p-toluenesulfonic acid, H₂O / acetone / 72 h

3: 1.) n-butyllithium / 1.) THF, -78 deg C, 2.) -78 deg C, 2 h

4: p-toluenesulfonic acid / acetone / 48 h / Ambient temperature

With n-butyllithium; water; potassium hydride; toluene-4-sulfonic acid; In acetone;
DOI:10.1021/jo00141a015

Reference yield:

: 2987-06-6
4-(benzyloxy)cyclohexanone

: 82732-16-9
4-(benzyloxy)-1-(3,4-dimethoxyphenyl)cyclohex-1-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-butyllithium / 1.) THF, -78 deg C, 2.) -78 deg C, 2 h

2: p-toluenesulfonic acid / acetone / 48 h / Ambient temperature

With n-butyllithium; toluene-4-sulfonic acid; In acetone;
DOI:10.1021/jo00141a015