9-(4-benzoylsulfanyl-5-methyl-1,3-dithiol-2-ylidene)-10-(4,5-dimethyl-1,3-dithiol-2-ylidene)-9,10-dihydroanthracene

Base Information

Chemical Name:9-(4-benzoylsulfanyl-5-methyl-1,3-dithiol-2-ylidene)-10-(4,5-dimethyl-1,3-dithiol-2-ylidene)-9,10-dihydroanthracene
CAS No.:224778-95-4
Molecular Formula:C₃₀H₂₂OS₅
Molecular Weight:558.834
Hs Code.:

Synonyms:9-(4-benzoylsulfanyl-5-methyl-1,3-dithiol-2-ylidene)-10-(4,5-dimethyl-1,3-dithiol-2-ylidene)-9,10-dihydroanthracene

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Chemical Property of 9-(4-benzoylsulfanyl-5-methyl-1,3-dithiol-2-ylidene)-10-(4,5-dimethyl-1,3-dithiol-2-ylidene)-9,10-dihydroanthracene

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Technology Process of 9-(4-benzoylsulfanyl-5-methyl-1,3-dithiol-2-ylidene)-10-(4,5-dimethyl-1,3-dithiol-2-ylidene)-9,10-dihydroanthracene

There total 2 articles about 9-(4-benzoylsulfanyl-5-methyl-1,3-dithiol-2-ylidene)-10-(4,5-dimethyl-1,3-dithiol-2-ylidene)-9,10-dihydroanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 98-88-4
benzoyl chloride

: 224778-82-9
9-(4,5-dimethyl-1,3-dithiol-2-ylidene)-10-(4-methyl-1,3-dithiol-2-ylidene)-9,10-dihydroanthracene

: 224778-95-4
9-(4-benzoylsulfanyl-5-methyl-1,3-dithiol-2-ylidene)-10-(4,5-dimethyl-1,3-dithiol-2-ylidene)-9,10-dihydroanthracene

Guidance literature:: With sulfur; lithium diisopropyl amide; In tetrahydrofuran; cyclohexane;
DOI:10.1002/(SICI)1099-0690(200001)2000:1<51::AID-EJOC51>3.0.CO;2-K

Reference yield:

: 128315-73-1
10-(4,5-Dimethyl-1,3-dithiol-2-ylidene)anthracene-9(10H)-one

: 224778-95-4
9-(4-benzoylsulfanyl-5-methyl-1,3-dithiol-2-ylidene)-10-(4,5-dimethyl-1,3-dithiol-2-ylidene)-9,10-dihydroanthracene

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / LDA / tetrahydrofuran / -78 - 20 °C

2: 53 percent / LDA; sulfur / tetrahydrofuran; cyclohexane

With sulfur; lithium diisopropyl amide; In tetrahydrofuran; cyclohexane; 1: Condensation / 2: Substitution;
DOI:10.1002/(SICI)1099-0690(200001)2000:1<51::AID-EJOC51>3.0.CO;2-K