[1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene]gold(III) trichloride

Base Information

Chemical Name:[1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene]gold(III) trichloride
CAS No.:1204354-69-7
Molecular Formula:C₂₇H₃₆AuCl₃N₂
Molecular Weight:691.922
Hs Code.:

Synonyms:[1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene]gold(III) trichloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene]gold(III) trichloride

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Technology Process of [1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene]gold(III) trichloride

There total 4 articles about [1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene]gold(III) trichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: chloro(1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene)gold(I)

: 932-72-9
(Dichloroiodo)benzene

: 1204354-69-7
[1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene]gold(III) trichloride

Guidance literature:: In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1002/ejoc.201200891

Reference yield:

: 74663-75-5,134750-23-5
1,2-bis(2,6-diisopropylphenylimino)ethane

: 1204354-69-7
[1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene]gold(III) trichloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride / toluene; diethyl ether / 41 h / 20 - 80 °C / Inert atmosphere

2.1: silver(l) oxide / dichloromethane / 3 h / 30 °C / Inert atmosphere

2.2: 3 h / 30 °C / Inert atmosphere

3.1: dichloromethane / 20 °C / Inert atmosphere

With hydrogenchloride; silver(l) oxide; In diethyl ether; dichloromethane; toluene;
DOI:10.1002/ejoc.201200891

Reference yield:

: 250285-32-6
1,3-bis[2,6-diisopropylphenyl]imidazolium chloride

: 1204354-69-7
[1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene]gold(III) trichloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: silver(l) oxide / dichloromethane / 3 h / 30 °C / Inert atmosphere

1.2: 3 h / 30 °C / Inert atmosphere

2.1: dichloromethane / 20 °C / Inert atmosphere

With silver(l) oxide; In dichloromethane;
DOI:10.1002/ejoc.201200891