{1-[2-(2-Methyl-cyclohexa-1,4-dienyl)-ethyl]-cyclohexa-2,4-dienyl}-methanol

Base Information

Chemical Name:{1-[2-(2-Methyl-cyclohexa-1,4-dienyl)-ethyl]-cyclohexa-2,4-dienyl}-methanol
CAS No.:110512-01-1
Molecular Formula:C₁₆H₂₂O
Molecular Weight:230.35
Hs Code.:

Synonyms:{1-[2-(2-Methyl-cyclohexa-1,4-dienyl)-ethyl]-cyclohexa-2,4-dienyl}-methanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of {1-[2-(2-Methyl-cyclohexa-1,4-dienyl)-ethyl]-cyclohexa-2,4-dienyl}-methanol

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Technology Process of {1-[2-(2-Methyl-cyclohexa-1,4-dienyl)-ethyl]-cyclohexa-2,4-dienyl}-methanol

There total 3 articles about {1-[2-(2-Methyl-cyclohexa-1,4-dienyl)-ethyl]-cyclohexa-2,4-dienyl}-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 110511-81-4
1-[2-(2-Methyl-cyclohexa-1,4-dienyl)-ethyl]-cyclohexa-2,4-dienecarboxylic acid methyl ester

: 110512-01-1
{1-[2-(2-Methyl-cyclohexa-1,4-dienyl)-ethyl]-cyclohexa-2,4-dienyl}-methanol

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; at -78 ℃; for 2.5h;
DOI:10.1021/ja00254a051

Reference yield:

: 110511-79-0
2-(2-methylcyclohexa-1,4-dien-1-yl)ethan-1-ol

: 110512-01-1
{1-[2-(2-Methyl-cyclohexa-1,4-dienyl)-ethyl]-cyclohexa-2,4-dienyl}-methanol

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / Ph₃P, imidazole, iodine / diethyl ether; acetonitrile / 0.5 h / 25 °C

2: 1.) LDA, 2.) hexamethylphosphoric triamide / 1.) THF, -78 deg C, 1 h, 2.) THF, -78 deg C, 5 h; -78 to -20 deg C, 9 h

3: 90 percent / diisobutylaluminum hydride / CH₂Cl₂ / 2.5 h / -78 °C

With 1H-imidazole; N,N,N,N,N,N-hexamethylphosphoric triamide; iodine; diisobutylaluminium hydride; triphenylphosphine; lithium diisopropyl amide; In diethyl ether; dichloromethane; acetonitrile;
DOI:10.1021/ja00254a051

Reference yield:

: 110511-80-3
1-(2-Iodo-ethyl)-2-methyl-cyclohexa-1,4-diene

: 110512-01-1
{1-[2-(2-Methyl-cyclohexa-1,4-dienyl)-ethyl]-cyclohexa-2,4-dienyl}-methanol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) LDA, 2.) hexamethylphosphoric triamide / 1.) THF, -78 deg C, 1 h, 2.) THF, -78 deg C, 5 h; -78 to -20 deg C, 9 h

2: 90 percent / diisobutylaluminum hydride / CH₂Cl₂ / 2.5 h / -78 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; diisobutylaluminium hydride; lithium diisopropyl amide; In dichloromethane;
DOI:10.1021/ja00254a051