ethyl 4-(4-iodo-3-trifluoromethylpyrazol-1-yl)-2-trifluoromethylbenzoate

Base Information

Chemical Name:ethyl 4-(4-iodo-3-trifluoromethylpyrazol-1-yl)-2-trifluoromethylbenzoate
CAS No.:1208356-32-4
Molecular Formula:C₁₄H₉F₆IN₂O₂
Molecular Weight:478.133
Hs Code.:

Synonyms:ethyl 4-(4-iodo-3-trifluoromethylpyrazol-1-yl)-2-trifluoromethylbenzoate

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Chemical Property of ethyl 4-(4-iodo-3-trifluoromethylpyrazol-1-yl)-2-trifluoromethylbenzoate

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Technology Process of ethyl 4-(4-iodo-3-trifluoromethylpyrazol-1-yl)-2-trifluoromethylbenzoate

There total 1 articles about ethyl 4-(4-iodo-3-trifluoromethylpyrazol-1-yl)-2-trifluoromethylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: ethyl 4-fluoro-2-trifluoromethylbenzoate

: 866638-72-4
4-iodo-3-(trifluoromethyl)-1H-pyrazole

: 1208356-32-4
ethyl 4-(4-iodo-3-trifluoromethylpyrazol-1-yl)-2-trifluoromethylbenzoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 1h;

Reference yield: 29.0%

: 1208356-32-4
ethyl 4-(4-iodo-3-trifluoromethylpyrazol-1-yl)-2-trifluoromethylbenzoate

: 67492-50-6
(3,5-dichlorophenyl)boronic acid

: 1208348-70-2
ethyl 4-[4-(3,5-dichlorophenyl)-3-trifluoromethylpyrazol-1-yl]-2-trifluoromethylbenzoate

Guidance literature:: With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; water; at 85 ℃; for 9h; Inert atmosphere;

Reference yield:

: 1208356-32-4
ethyl 4-(4-iodo-3-trifluoromethylpyrazol-1-yl)-2-trifluoromethylbenzoate

: 1208348-71-3
4-[4-(3,5-dichlorophenyl)-3-trifluoromethylpyrazol-1-yl]-2-trifluoromethylbenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 9 h / 85 °C / Inert atmosphere

2: water; sodium hydroxide / ethanol / 20 °C

With water; potassium carbonate; sodium hydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; ethanol; water;