β-lactone of 2-carboxy-3-hydroxy-2-methyl-2',4',7-trimethoxy-2,3-dihydroisoflavone

Base Information

Chemical Name:β-lactone of 2-carboxy-3-hydroxy-2-methyl-2',4',7-trimethoxy-2,3-dihydroisoflavone
CAS No.:113180-58-8
Molecular Formula:C₂₀H₁₈O₇
Molecular Weight:370.359
Hs Code.:

Synonyms:β-lactone of 2-carboxy-3-hydroxy-2-methyl-2',4',7-trimethoxy-2,3-dihydroisoflavone

Suppliers and Price of β-lactone of 2-carboxy-3-hydroxy-2-methyl-2',4',7-trimethoxy-2,3-dihydroisoflavone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of β-lactone of 2-carboxy-3-hydroxy-2-methyl-2',4',7-trimethoxy-2,3-dihydroisoflavone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of β-lactone of 2-carboxy-3-hydroxy-2-methyl-2',4',7-trimethoxy-2,3-dihydroisoflavone

There total 6 articles about β-lactone of 2-carboxy-3-hydroxy-2-methyl-2',4',7-trimethoxy-2,3-dihydroisoflavone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₀H₁₉ClO₈

: 113180-58-8
β-lactone of 2-carboxy-3-hydroxy-2-methyl-2',4',7-trimethoxy-2,3-dihydroisoflavone

Guidance literature:: With triethylamine; In benzene; at 50 ℃; Yield given;
DOI:10.1021/jo00242a002

Reference yield:

: 6706-94-1
2,2'-hydroxy-4,4'-methoxybenzil

: 113180-58-8
β-lactone of 2-carboxy-3-hydroxy-2-methyl-2',4',7-trimethoxy-2,3-dihydroisoflavone

Guidance literature:: Multi-step reaction with 5 steps

1: K₂CO₃

2: K₂CO₃ / acetone / 9 h / Heating

3: KOH / aq. ethanol

4: oxalyl chloride / benzene

5: triethylamine / benzene / 50 °C

With potassium hydroxide; oxalyl dichloride; potassium carbonate; triethylamine; In ethanol; acetone; benzene;
DOI:10.1021/jo00242a002

Reference yield:

: 95281-05-3
2-Hydroxy-4,2',4'-trimethoxy-benzil

: 113180-58-8
β-lactone of 2-carboxy-3-hydroxy-2-methyl-2',4',7-trimethoxy-2,3-dihydroisoflavone

Guidance literature:: Multi-step reaction with 4 steps

1: K₂CO₃ / acetone / 9 h / Heating

2: KOH / aq. ethanol

3: oxalyl chloride / benzene

4: triethylamine / benzene / 50 °C

With potassium hydroxide; oxalyl dichloride; potassium carbonate; triethylamine; In ethanol; acetone; benzene;
DOI:10.1021/jo00242a002