benzoaza-12-crown-4

Base Information

Chemical Name:benzoaza-12-crown-4
CAS No.:41536-50-9
Molecular Formula:C₁₂H₁₇NO₃
Molecular Weight:223.272
Hs Code.:

Synonyms:benzoaza-12-crown-4

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzoaza-12-crown-4

Chemical Property:

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Technology Process of benzoaza-12-crown-4

There total 3 articles about benzoaza-12-crown-4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 112-26-5,27252-69-3
1,2-bis(2-chloroethoxy)ethane

: 95-55-6
2-amino-phenol

: 41536-50-9
benzoaza-12-crown-4

: C₂₄H₃₄N₂O₆

: 2-{2-[2-(2-chloroethoxy)ethoxy]ethoxy}aniline

: 2-{2-[2-(2-chloroethoxy)ethoxy]ethoxy}-N-{2-[2-(2-chloroethoxy)ethoxy]ethyl}aniline

Guidance literature:: 2-amino-phenol; With sodium hydroxide; In isopropyl alcohol; at 60 ℃; for 1h;

1,2-bis(2-chloroethoxy)ethane; In isopropyl alcohol; for 20h; Reflux;
DOI:10.1134/S107036321411005X

Reference yield: 20.1%

: 112-26-5,27252-69-3
1,2-bis(2-chloroethoxy)ethane

: 95-55-6
2-amino-phenol

: 71-36-3
butan-1-ol

: 41536-50-9
benzoaza-12-crown-4

: 2-{2-[2-(2-chloroethoxy)ethoxy]ethoxy}-N-{2-[2-(2-chloroethoxy)ethoxy]ethyl}aniline

: 63512-36-7,31885-97-9
α-butyl-ω-butoxymono-tris-oxyethylene

: 52184-05-1
1-{2-[2-(2-chloroethoxy)ethoxy]ethoxy}butane

Guidance literature:: 2-amino-phenol; With sodium hydroxide; In butan-1-ol; at 80 ℃; for 1h; Sonication;

1,2-bis(2-chloroethoxy)ethane; butan-1-ol; for 20h; Reflux;
DOI:10.1134/S107036321411005X

Reference yield: 14.0%

: 95-55-6
2-amino-phenol

: 19249-03-7
triethylene glycol di-(p-toluenesulfonate)

: 41536-50-9
benzoaza-12-crown-4

Guidance literature:: 2-amino-phenol; With cesium fluoride; In acetonitrile; for 1h;

triethylene glycol di-(p-toluenesulfonate); In acetonitrile; for 16h; Heating / reflux;