6-Chloropyridine-2-carboxylic acid amide

Base Information

• Chemical Name: 6-Chloropyridine-2-carboxylic acid amide
• CAS No.: 7059-61-2
• Molecular Formula: C₂₄H₁₆F₂O₂
• Molecular Weight: 374.387
• Mol file: 7059-61-2.mol

Synonyms:1,3-Bis-<3-(4-fluor-phenyl)-3-oxo-prop-1-enyl>-benzol

Chemical Property of 6-Chloropyridine-2-carboxylic acid amide

Chemical Property:

• Melting Point: 190-191 °C
• Boiling Point: 554.7±50.0 °C(Predicted)
• Density: 1.253±0.06 g/cm3(Predicted)

Purity/Quality:

98%min ^*data from raw suppliers

6-Chloropyridine-2-carboxylic acid amide Aldrich ^*data from reagent suppliers

Safty Information:

• Statements: 43
• Safety Statements: 36/37

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-Chloropyridine-2-carboxylic acid amide

There total 1 articles about 6-Chloropyridine-2-carboxylic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 1,3-Bis-<3-(4-fluor-phenyl)-3-oxo-prop-1-enyl>-benzol (7059-61-2)

Guidance literature:

m-Phthalaldehyd, 1-<4-Fluor-phenyl>-ethanon, Me., methanol. KOH;

Reference yield:

1,3-Bis-<3-(4-fluor-phenyl)-3-oxo-prop-1-enyl>-benzol (7059-61-2) + diphenylphosphane (829-85-6) → C48H38F2O2P2 (1335292-77-7)

Guidance literature:

diphenylphosphane; With C₂₉H₂₆N₂Pd⁽¹⁺⁾*ClO₄^(1-); In toluene; at 20 ℃; for 0.166667h; Inert atmosphere;

1,3-Bis-<3-(4-fluor-phenyl)-3-oxo-prop-1-enyl>-benzol; With triethylamine; In toluene; at -80 ℃; for 45h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;

DOI:10.1021/ol202480r

Downstream raw materials:

C₄₈H₃₈F₂O₂P₂

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