Valin-N-(4-methylphenyl)hydroxamsaeure

Base Information

Chemical Name:Valin-N-(4-methylphenyl)hydroxamsaeure
CAS No.:126875-70-5
Molecular Formula:C₁₂H₁₈N₂O₂
Molecular Weight:222.287
Hs Code.:

Synonyms:Valin-N-(4-methylphenyl)hydroxamsaeure

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Chemical Property of Valin-N-(4-methylphenyl)hydroxamsaeure

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Technology Process of Valin-N-(4-methylphenyl)hydroxamsaeure

There total 4 articles about Valin-N-(4-methylphenyl)hydroxamsaeure which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 126901-04-0
(S)-2-(1,3-Dioxo-1,3-dihydro-isoindol-2-yl)-N-hydroxy-3-methyl-N-p-tolyl-butyramide

: 126875-70-5
Valin-N-(4-methylphenyl)hydroxamsaeure

Guidance literature:: With hydrazine hydrate; In ethanol; for 2h; Heating;

Reference yield:

: 72-18-4,25609-85-2,7004-03-7,921-10-8
L-valine

: 126875-70-5
Valin-N-(4-methylphenyl)hydroxamsaeure

Guidance literature:: Multi-step reaction with 4 steps

1: 0.5 h / 150 - 180 °C

2: PCl₅ / benzene / 1 h

3: NaHCO₃ / diethyl ether / 12 h / -78 deg C -> 25 deg C

4: 95 percent / N₂H₄*H₂O / ethanol / 2 h / Heating

With phosphorus pentachloride; sodium hydrogencarbonate; hydrazine hydrate; In diethyl ether; ethanol; benzene;

Reference yield:

: 5511-73-9
N-phthalimide l-valinyl chloride

: 126875-70-5
Valin-N-(4-methylphenyl)hydroxamsaeure

Guidance literature:: Multi-step reaction with 2 steps

1: NaHCO₃ / diethyl ether / 12 h / -78 deg C -> 25 deg C

2: 95 percent / N₂H₄*H₂O / ethanol / 2 h / Heating

With sodium hydrogencarbonate; hydrazine hydrate; In diethyl ether; ethanol;