Technology Process of 1-(ethenyloxy)-2-(methoxymethyl)benzene
There total 5 articles about 1-(ethenyloxy)-2-(methoxymethyl)benzene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
DBN; silver perchlorate;
In
methanol;
for 1h;
Ambient temperature;
DOI:10.1021/ja00010a038
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 57 percent / potassium tert-butoxide / dimethylsulfoxide / 0.25 h / Ambient temperature
2: 85 percent / LiAlH4 / diethyl ether / 1 h / Heating
3: triphenylphosphine / dimethylformamide / 1 h / 30 °C
4: 84.3 percent / 1,5-diazabicyclo<4.3.0>non-5-ene (DBN), AgClO4 / methanol / 1 h / Ambient temperature
With
lithium aluminium tetrahydride; DBN; potassium tert-butylate; silver perchlorate; triphenylphosphine;
In
methanol; diethyl ether; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/ja00010a038
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 85 percent / LiAlH4 / diethyl ether / 1 h / Heating
2: triphenylphosphine / dimethylformamide / 1 h / 30 °C
3: 84.3 percent / 1,5-diazabicyclo<4.3.0>non-5-ene (DBN), AgClO4 / methanol / 1 h / Ambient temperature
With
lithium aluminium tetrahydride; DBN; silver perchlorate; triphenylphosphine;
In
methanol; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1021/ja00010a038