ethyl N-[2,3,5-trichloro-4-(4-hydroxy-3-isopropylphenoxy)phenyl]malonamate

Base Information

Chemical Name:ethyl N-[2,3,5-trichloro-4-(4-hydroxy-3-isopropylphenoxy)phenyl]malonamate
CAS No.:373641-40-8
Molecular Formula:C₂₀H₂₀Cl₃NO₅
Molecular Weight:460.742
Hs Code.:

Synonyms:ethyl N-[2,3,5-trichloro-4-(4-hydroxy-3-isopropylphenoxy)phenyl]malonamate

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Chemical Property of ethyl N-[2,3,5-trichloro-4-(4-hydroxy-3-isopropylphenoxy)phenyl]malonamate

Chemical Property:

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Technology Process of ethyl N-[2,3,5-trichloro-4-(4-hydroxy-3-isopropylphenoxy)phenyl]malonamate

There total 6 articles about ethyl N-[2,3,5-trichloro-4-(4-hydroxy-3-isopropylphenoxy)phenyl]malonamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 373643-21-1
ethyl n-[4-(4-benzyloxy-3-isopropylphenoxy)-2,3,5-trichlorophenyl]malonamate

: 373641-40-8
ethyl N-[2,3,5-trichloro-4-(4-hydroxy-3-isopropylphenoxy)phenyl]malonamate

Guidance literature:: With dimethylsulfide; water; trifluoroacetic acid; at 20 ℃;
DOI:10.1016/j.bmc.2012.03.056

Reference yield:

: bis(4-benzyloxy-3-isopropylphenyl)iodonium tetrafluoroborate

: 373641-40-8
ethyl N-[2,3,5-trichloro-4-(4-hydroxy-3-isopropylphenoxy)phenyl]malonamate

Guidance literature:: Multi-step reaction with 4 steps

1: bronze powder; triethylamine / dichloromethane / 120 h / 20 °C

2: platinum(IV) oxide; hydrogen / ethyl acetate / 2 h / 20 °C

3: pyridine / dichloromethane / 3 h / 0 - 20 °C

4: dimethylsulfide; water; trifluoroacetic acid / 20 °C

With pyridine; platinum(IV) oxide; bronze powder; dimethylsulfide; water; hydrogen; triethylamine; trifluoroacetic acid; In dichloromethane; ethyl acetate;
DOI:10.1016/j.bmc.2012.03.056

Reference yield:

: 88-69-7
2-(1-methylethyl)phenol

: 373641-40-8
ethyl N-[2,3,5-trichloro-4-(4-hydroxy-3-isopropylphenoxy)phenyl]malonamate

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium carbonate / acetonitrile / 29 h / Reflux

2.1: iodine tris(trifluoroacetate); acetic anhydride; trifluoroacetic acid / 16 h / 4 °C

2.2: 0.5 h

3.1: bronze powder; triethylamine / dichloromethane / 120 h / 20 °C

4.1: platinum(IV) oxide; hydrogen / ethyl acetate / 2 h / 20 °C

5.1: pyridine / dichloromethane / 3 h / 0 - 20 °C

6.1: dimethylsulfide; water; trifluoroacetic acid / 20 °C

With pyridine; platinum(IV) oxide; bronze powder; dimethylsulfide; iodine tris(trifluoroacetate); water; hydrogen; acetic anhydride; potassium carbonate; triethylamine; trifluoroacetic acid; In dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1016/j.bmc.2012.03.056