2,3,4-tri-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-6-O-trityl-β-D-glucopyranosylamine

Base Information

Chemical Name:2,3,4-tri-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-6-O-trityl-β-D-glucopyranosylamine
CAS No.:144310-53-2
Molecular Formula:C₅₄H₄₉NO₁₂
Molecular Weight:903.983
Hs Code.:

Synonyms:2,3,4-tri-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-6-O-trityl-β-D-glucopyranosylamine

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Chemical Property of 2,3,4-tri-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-6-O-trityl-β-D-glucopyranosylamine

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Technology Process of 2,3,4-tri-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-6-O-trityl-β-D-glucopyranosylamine

There total 3 articles about 2,3,4-tri-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-6-O-trityl-β-D-glucopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 98-88-4
benzoyl chloride

: 144310-50-9
N-(2,2-diethoxycarbonylvinyl)-6-O-trityl-β-D-glucopyranosylamine

: 144310-53-2
2,3,4-tri-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-6-O-trityl-β-D-glucopyranosylamine

Guidance literature:: With pyridine;
DOI:10.1016/S0008-6215(00)90993-5

Reference yield:

: 22435-63-8
N-(2,2-diethoxycarbonylvinyl)-β-D-glucopyranosylamine

: 144310-53-2
2,3,4-tri-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-6-O-trityl-β-D-glucopyranosylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / pyridine / 24 h / 50 °C

2: 67 percent / pyridine

With pyridine;
DOI:10.1016/S0008-6215(00)90993-5

Reference yield:

: 76-83-5
trityl chloride

: 144310-53-2
2,3,4-tri-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-6-O-trityl-β-D-glucopyranosylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / pyridine / 24 h / 50 °C

2: 67 percent / pyridine

With pyridine;
DOI:10.1016/S0008-6215(00)90993-5