N-(but-1-en-3-yl)-6-ethenyl-2-methoxy-N-p-toluenesulfonylaniline

Base Information

Chemical Name:N-(but-1-en-3-yl)-6-ethenyl-2-methoxy-N-p-toluenesulfonylaniline
CAS No.:1192805-29-0
Molecular Formula:C₂₀H₂₃NO₃S
Molecular Weight:357.474
Hs Code.:

Synonyms:N-(but-1-en-3-yl)-6-ethenyl-2-methoxy-N-p-toluenesulfonylaniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(but-1-en-3-yl)-6-ethenyl-2-methoxy-N-p-toluenesulfonylaniline

Chemical Property:

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Technology Process of N-(but-1-en-3-yl)-6-ethenyl-2-methoxy-N-p-toluenesulfonylaniline

There total 1 articles about N-(but-1-en-3-yl)-6-ethenyl-2-methoxy-N-p-toluenesulfonylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 894810-79-8
N-p-toluenesulfonyl-2-ethenyl-6-methoxyaniline

: 598-32-3
2-hydroxy-3-butene

: 1192805-29-0
N-(but-1-en-3-yl)-6-ethenyl-2-methoxy-N-p-toluenesulfonylaniline

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 20 ℃; for 2.5h;
DOI:10.1002/ejoc.200900520

Reference yield: 92.0%

: 1192805-29-0
N-(but-1-en-3-yl)-6-ethenyl-2-methoxy-N-p-toluenesulfonylaniline

: 1192805-50-7
C₁₇H₁₇NO₃S

Guidance literature:: N-(but-1-en-3-yl)-6-ethenyl-2-methoxy-N-p-toluenesulfonylaniline; With carbonylchlorohydridotris(triphenylphosphine)ruthenium(II); for 4h; Reflux;

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; for 3h; Reflux;
DOI:10.1021/jm301084z

Reference yield:

: 1192805-29-0
N-(but-1-en-3-yl)-6-ethenyl-2-methoxy-N-p-toluenesulfonylaniline

: 1398631-78-1
C₂₆H₂₂ClNO₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: carbonylchlorohydridotris(triphenylphosphine)ruthenium(II) / 4 h / Reflux

1.2: 3 h / Reflux

2.1: potassium hydroxide / methanol / 4 h / Reflux

3.1: n-butyllithium; zinc(II) chloride / tetrahydrofuran; hexane; diethyl ether / 1 h / 0 - 20 °C

3.2: 15 h

4.1: potassium tert-butylate / tetrahydrofuran / 1 h / -78 °C

4.2: 3 h

With carbonylchlorohydridotris(triphenylphosphine)ruthenium(II); n-butyllithium; potassium tert-butylate; potassium hydroxide; zinc(II) chloride; In tetrahydrofuran; methanol; diethyl ether; hexane;
DOI:10.1021/jm301084z