C₄₀H₄₄N₄O₉Si

Base Information

Chemical Name:C₄₀H₄₄N₄O₉Si
CAS No.:1027505-70-9
Molecular Formula:C₄₀H₄₄N₄O₉Si
Molecular Weight:752.896
Hs Code.:

C<sub>40</sub>H<sub>44</sub>N<sub>4</sub>O<sub>9</sub>Si

Synonyms:C₄₀H₄₄N₄O₉Si

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Chemical Property of C₄₀H₄₄N₄O₉Si

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Technology Process of C₄₀H₄₄N₄O₉Si

There total 11 articles about C₄₀H₄₄N₄O₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1025823-46-4
C₄₀H₄₆N₄O₉Si

: 1027505-70-9
C₄₀H₄₄N₄O₉Si

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane;
DOI:10.3987/COM-02-S42

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1027505-70-9
C₄₀H₄₄N₄O₉Si

Guidance literature:: Multi-step reaction with 6 steps

1: 85 percent / imidazole / CH₂Cl₂ / 20 °C

2: 80 percent / H₂ / Pd/C / ethyl acetate

3: DCC; HOAt / tetrahydrofuran / 20 °C

4: 100 percent / TEA; DMAP / CH₂Cl₂

5: 89 percent / DDQ / CH₂Cl₂; H₂O / 20 °C

6: 96 percent / DMSO; (COCl)2; Et₃N / CH₂Cl₂

With 1H-imidazole; dmap; 1-hydroxy-7-aza-benzotriazole; oxalyl dichloride; TEA; hydrogen; dimethyl sulfoxide; triethylamine; dicyclohexyl-carbodiimide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; water; ethyl acetate; 6: Swern oxidation;
DOI:10.3987/COM-02-S42

Reference yield:

: 193893-12-8
(2R,3S)-3-Azido-4-(tert-butyl-diphenyl-silanyloxy)-1-(4-methoxy-benzyloxy)-butan-2-ol

: 1027505-70-9
C₄₀H₄₄N₄O₉Si

Guidance literature:: Multi-step reaction with 5 steps

1: 80 percent / H₂ / Pd/C / ethyl acetate

2: DCC; HOAt / tetrahydrofuran / 20 °C

3: 100 percent / TEA; DMAP / CH₂Cl₂

4: 89 percent / DDQ / CH₂Cl₂; H₂O / 20 °C

5: 96 percent / DMSO; (COCl)2; Et₃N / CH₂Cl₂

With dmap; 1-hydroxy-7-aza-benzotriazole; oxalyl dichloride; TEA; hydrogen; dimethyl sulfoxide; triethylamine; dicyclohexyl-carbodiimide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; water; ethyl acetate; 5: Swern oxidation;
DOI:10.3987/COM-02-S42