Technology Process of C15H21NO4
There total 4 articles about C15H21NO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylsilane; trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
for 4h;
Inert atmosphere;
DOI:10.1021/np100877h
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: silver benzoate; triethylamine / 4 h / 70 °C / Darkness; Inert atmosphere
2.1: n-butyllithium; diisopropylamine; lithium chloride / tetrahydrofuran; hexane / 1 h
2.2: 21 h / 20 °C
3.1: triethylsilane; trifluoroacetic acid / dichloromethane / 4 h / 20 °C / Inert atmosphere
With
triethylsilane; n-butyllithium; silver benzoate; triethylamine; diisopropylamine; trifluoroacetic acid; lithium chloride;
In
tetrahydrofuran; hexane; dichloromethane;
1.1: Wolff rearrangement;
DOI:10.1021/np100877h
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: chloroformic acid ethyl ester; triethylamine / tetrahydrofuran / 0.5 h / -15 °C / Inert atmosphere
1.2: 18 h / 0 - 20 °C / Inert atmosphere
2.1: silver benzoate; triethylamine / 4 h / 70 °C / Darkness; Inert atmosphere
3.1: n-butyllithium; diisopropylamine; lithium chloride / tetrahydrofuran; hexane / 1 h
3.2: 21 h / 20 °C
4.1: triethylsilane; trifluoroacetic acid / dichloromethane / 4 h / 20 °C / Inert atmosphere
With
triethylsilane; n-butyllithium; silver benzoate; chloroformic acid ethyl ester; triethylamine; diisopropylamine; trifluoroacetic acid; lithium chloride;
In
tetrahydrofuran; hexane; dichloromethane;
1.1: Arndt-Eistert reaction / 1.2: Arndt-Eistert reaction / 2.1: Wolff rearrangement;
DOI:10.1021/np100877h
