p-methoxyphenyl (2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-(1->3)-4,6-O-benzylidene-2-deoxy-2-N-phthalimido-β-D-glucopyranoside

Base Information

Chemical Name:p-methoxyphenyl (2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-(1->3)-4,6-O-benzylidene-2-deoxy-2-N-phthalimido-β-D-glucopyranoside
CAS No.:1393114-53-8
Molecular Formula:C₄₆H₅₁N₃O₁₄
Molecular Weight:869.923
Hs Code.:

Synonyms:p-methoxyphenyl (2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-(1->3)-4,6-O-benzylidene-2-deoxy-2-N-phthalimido-β-D-glucopyranoside

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Chemical Property of p-methoxyphenyl (2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-(1->3)-4,6-O-benzylidene-2-deoxy-2-N-phthalimido-β-D-glucopyranoside

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Technology Process of p-methoxyphenyl (2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-(1->3)-4,6-O-benzylidene-2-deoxy-2-N-phthalimido-β-D-glucopyranoside

There total 1 articles about p-methoxyphenyl (2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-(1->3)-4,6-O-benzylidene-2-deoxy-2-N-phthalimido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 869107-36-8
4-methoxyphenyl 2,3,6-tri-O-benzyl-β-D-galactopyranoside

: 83025-20-1
3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-galactopyranosyltrichloroacetimidate

: 1393114-53-8
p-methoxyphenyl (2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-(1->3)-4,6-O-benzylidene-2-deoxy-2-N-phthalimido-β-D-glucopyranoside

Guidance literature:: With perchloric acid supported over silica; In diethyl ether; dichloromethane; at -20 ℃; for 1h; stereoselective reaction;
DOI:10.1007/s10719-012-9383-4

Reference yield:

: 1393114-53-8
p-methoxyphenyl (2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-(1->3)-4,6-O-benzylidene-2-deoxy-2-N-phthalimido-β-D-glucopyranoside

: C₄₀H₄₅N₃O₁₁

Guidance literature:: With sodium methylate; In methanol; at 20 ℃; for 2h;
DOI:10.1007/s10719-012-9383-4

Reference yield:

: 1393114-53-8
p-methoxyphenyl (2-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-(1->3)-4,6-O-benzylidene-2-deoxy-2-N-phthalimido-β-D-glucopyranoside

: 1393114-55-0
p-methoxyphenyl (2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1->3)-(4,6-O-benzylidene-2-azido-2-deoxy-α-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium methylate / methanol / 2 h / 20 °C

2.1: perchloric acid supported over silica / N,N-dimethyl-formamide; acetonitrile / 5 h / 20 °C

3.1: dichloromethane / 0.5 h / 20 °C / Inert atmosphere; Molecular sieve

3.2: perchloric acid supported silica / 0.75 h / -40 °C / Inert atmosphere

With sodium methylate; In methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1007/s10719-012-9383-4