(1S,2R)-2-benzyloxymethylcyclopropyl phenyl sulfone

Base Information

Chemical Name:(1S,2R)-2-benzyloxymethylcyclopropyl phenyl sulfone
CAS No.:1233934-54-7
Molecular Formula:C₁₇H₁₈O₃S
Molecular Weight:302.394
Hs Code.:

Synonyms:(1S,2R)-2-benzyloxymethylcyclopropyl phenyl sulfone

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Chemical Property of (1S,2R)-2-benzyloxymethylcyclopropyl phenyl sulfone

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Technology Process of (1S,2R)-2-benzyloxymethylcyclopropyl phenyl sulfone

There total 1 articles about (1S,2R)-2-benzyloxymethylcyclopropyl phenyl sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 56069-39-7
diethyl phenylsulfonylmethylphosphonate

: 2930-05-4,14618-80-5,89616-40-0,16495-13-9
(S)-benzyl glycidyl ether

: 1233934-54-7
(1S,2R)-2-benzyloxymethylcyclopropyl phenyl sulfone

Guidance literature:: diethyl phenylsulfonylmethylphosphonate; With sodium hydride; In 1,2-dimethoxyethane; at 25 ℃;

(S)-benzyl glycidyl ether; In 1,2-dimethoxyethane; at 140 ℃; diastereoselective reaction;
DOI:10.1021/jo100844g

Reference yield: 65.0%

: 4206-67-1
iodo(trimethylsilyl)methane

: 1233934-54-7
(1S,2R)-2-benzyloxymethylcyclopropyl phenyl sulfone

: 139242-80-1
1-phenylsulfonyl-1-trimethylsilylmethyl-2-benzyloxymethylcyclopropane

Guidance literature:: (1S,2R)-2-benzyloxymethylcyclopropyl phenyl sulfone; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.533333h;

iodo(trimethylsilyl)methane; In tetrahydrofuran; at -78 - 20 ℃; for 3.03333h;
DOI:10.1021/jo100844g