N-[(9H-fluorenyl-9-ylmethoxy)carbonyl]-L-alanyl-N-(3,4-dimethoxyphenethyl)glycine allyl ester

Base Information

Chemical Name:N-[(9H-fluorenyl-9-ylmethoxy)carbonyl]-L-alanyl-N-(3,4-dimethoxyphenethyl)glycine allyl ester
CAS No.:916598-60-2
Molecular Formula:C₃₃H₃₆N₂O₇
Molecular Weight:572.658
Hs Code.:

Synonyms:N-[(9H-fluorenyl-9-ylmethoxy)carbonyl]-L-alanyl-N-(3,4-dimethoxyphenethyl)glycine allyl ester

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Chemical Property of N-[(9H-fluorenyl-9-ylmethoxy)carbonyl]-L-alanyl-N-(3,4-dimethoxyphenethyl)glycine allyl ester

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Technology Process of N-[(9H-fluorenyl-9-ylmethoxy)carbonyl]-L-alanyl-N-(3,4-dimethoxyphenethyl)glycine allyl ester

There total 2 articles about N-[(9H-fluorenyl-9-ylmethoxy)carbonyl]-L-alanyl-N-(3,4-dimethoxyphenethyl)glycine allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 916598-58-8
(3,4-dimethoxy-phenethylamino)acetic acid allyl ester

: 35661-39-3,136132-75-7
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine

: 916598-60-2
N-[(9H-fluorenyl-9-ylmethoxy)carbonyl]-L-alanyl-N-(3,4-dimethoxyphenethyl)glycine allyl ester

Guidance literature:: N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine; With 4-methyl-morpholine; isobutyl chloroformate; In N,N-dimethyl-formamide; at 0 ℃; for 0.166667h;

(3,4-dimethoxy-phenethylamino)acetic acid allyl ester; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/ol0622211

Reference yield:

: 40630-84-0
allyl bromoacetate

: 916598-60-2
N-[(9H-fluorenyl-9-ylmethoxy)carbonyl]-L-alanyl-N-(3,4-dimethoxyphenethyl)glycine allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 86 percent / Et₃N / CH₂Cl₂

2.1: 4-methylmorpholine; isobutyl chloroformate / dimethylformamide / 0.17 h / 0 °C

2.2: 100 percent / dimethylformamide / 20 °C

With 4-methyl-morpholine; triethylamine; isobutyl chloroformate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol0622211

Reference yield: 86.0%

: 916598-60-2
N-[(9H-fluorenyl-9-ylmethoxy)carbonyl]-L-alanyl-N-(3,4-dimethoxyphenethyl)glycine allyl ester

: N-[(9H-fluorenyl-9-ylmethoxy)carbonyl]-L-alanyl-N-(3,4-dimethoxyphenethyl)glycine

Guidance literature:: With morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 20 ℃; for 0.5h;
DOI:10.1021/ol0622211