[Rh(CO)(CH₃OC₅H₄NO)(P(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[Rh(CO)(CH₃OC₅H₄NO)(P(C₆H₅)3)2]ClO₄

Base Information

• Chemical Name: [Rh(CO)(CH₃OC₅H₄NO)(P(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[Rh(CO)(CH₃OC₅H₄NO)(P(C₆H₅)3)2]ClO₄
• CAS No.: 84190-73-8
• Molecular Formula: C₄₃H₃₇NO₃P₂Rh*ClO₄
• Molecular Weight: 880.075

Synonyms:[Rh(CO)(CH₃OC₅H₄NO)(P(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[Rh(CO)(CH₃OC₅H₄NO)(P(C₆H₅)3)2]ClO₄

Chemical Property of [Rh(CO)(CH₃OC₅H₄NO)(P(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[Rh(CO)(CH₃OC₅H₄NO)(P(C₆H₅)3)2]ClO₄

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Technology Process of [Rh(CO)(CH₃OC₅H₄NO)(P(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[Rh(CO)(CH₃OC₅H₄NO)(P(C₆H₅)3)2]ClO₄

There total 2 articles about [Rh(CO)(CH₃OC₅H₄NO)(P(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[Rh(CO)(CH₃OC₅H₄NO)(P(C₆H₅)3)2]ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

[Rh((CHCHC2H4)2)(ONC5H4OCH3)2](1+)*ClO4(1-)=[Rh((CHCHC2H4)2)(ONC5H4OCH3)2]ClO4 (80005-65-8) → [Rh(CO)(CH3OC5H4NO)(P(C6H5)3)2](1+)*ClO4(1-)=[Rh(CO)(CH3OC5H4NO)(P(C6H5)3)2]ClO4 (84190-73-8)

Guidance literature:

With CO; PPh₃; In dichloromethane; CO bubbled through complex soln. at room temp., PPh3 added, stirred for30 min; pptd. (ether); elem. anal.;

DOI:10.1016/S0022-328X(00)85856-8

Reference yield:

4-methoxypyridine N-oxide (1122-96-9) + [CO(P(C6H5)3)2RhCH3COCH3](1+)*ClO4(1-) = [CO(P(C6H5)3)2RhCH3COCH3]ClO4 (75214-93-6,32334-51-3) → [Rh(CO)(CH3OC5H4NO)(P(C6H5)3)2](1+)*ClO4(1-)=[Rh(CO)(CH3OC5H4NO)(P(C6H5)3)2]ClO4 (84190-73-8)

Guidance literature:

In acetone; stoich. amt. of ligand added to complex soln. at room temp.; concd., pptd. with ether, filtered off, washed with hexane or ether, dried (vac.);

DOI:10.1016/S0022-328X(00)85856-8

upstream raw materials:

4-methoxypyridine N-oxide

[CO(P(C₆H₅)3)2RhCH₃COCH₃]⁽¹⁺⁾*ClO₄^(1-) = [CO(P(C₆H₅)3)2RhCH₃COCH₃]ClO₄

[Rh((CHCHC₂H₄)2)(ONC₅H₄OCH₃)2]⁽¹⁺⁾*ClO₄^(1-)=[Rh((CHCHC₂H₄)2)(ONC₅H₄OCH₃)2]ClO₄

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