6-acetyl-4-(4-chlorophenyl)-2-ethoxycarbonyl-1,2,3,4-tetrahydro-1,2,4,5-tetrazine

Base Information

Chemical Name:6-acetyl-4-(4-chlorophenyl)-2-ethoxycarbonyl-1,2,3,4-tetrahydro-1,2,4,5-tetrazine
CAS No.:216169-52-7
Molecular Formula:C₁₃H₁₅ClN₄O₃
Molecular Weight:310.74
Hs Code.:

Synonyms:6-acetyl-4-(4-chlorophenyl)-2-ethoxycarbonyl-1,2,3,4-tetrahydro-1,2,4,5-tetrazine

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Chemical Property of 6-acetyl-4-(4-chlorophenyl)-2-ethoxycarbonyl-1,2,3,4-tetrahydro-1,2,4,5-tetrazine

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Technology Process of 6-acetyl-4-(4-chlorophenyl)-2-ethoxycarbonyl-1,2,3,4-tetrahydro-1,2,4,5-tetrazine

There total 4 articles about 6-acetyl-4-(4-chlorophenyl)-2-ethoxycarbonyl-1,2,3,4-tetrahydro-1,2,4,5-tetrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 216169-46-9
1-ethoxycarbonyl-1-methyl-2-[1-(4-chlorophenyl)hydrazonopropan-2-one]hydrazine

: 216169-52-7
6-acetyl-4-(4-chlorophenyl)-2-ethoxycarbonyl-1,2,3,4-tetrahydro-1,2,4,5-tetrazine

Guidance literature:: With pyrographite; In toluene; at 110 ℃; for 4h;

Reference yield:

: C₉H₇ClN₂O

: 216169-52-7
6-acetyl-4-(4-chlorophenyl)-2-ethoxycarbonyl-1,2,3,4-tetrahydro-1,2,4,5-tetrazine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 0 - 20 °C

2: pyrographite / toluene / 4 h / 110 °C

With pyrographite; In tetrahydrofuran; toluene;

Reference yield:

: 2028-74-2
p-chlorobenzenediazonium chloride

: 216169-52-7
6-acetyl-4-(4-chlorophenyl)-2-ethoxycarbonyl-1,2,3,4-tetrahydro-1,2,4,5-tetrazine

Guidance literature:: Multi-step reaction with 4 steps

2: triethylamine / tetrahydrofuran / 0 °C

3: tetrahydrofuran / 0 - 20 °C

4: pyrographite / toluene / 4 h / 110 °C

With pyrographite; triethylamine; In tetrahydrofuran; toluene; 1: Japp-Klingemann reaction;