(S,E)-benzyl 8-(tert-butyldiphenylsilyloxy)-2-methyloct-5-en-4-ylcarbamate

Base Information

Chemical Name:(S,E)-benzyl 8-(tert-butyldiphenylsilyloxy)-2-methyloct-5-en-4-ylcarbamate
CAS No.:1205536-91-9
Molecular Formula:C₃₃H₄₃NO₃Si
Molecular Weight:529.795
Hs Code.:

Synonyms:(S,E)-benzyl 8-(tert-butyldiphenylsilyloxy)-2-methyloct-5-en-4-ylcarbamate

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Chemical Property of (S,E)-benzyl 8-(tert-butyldiphenylsilyloxy)-2-methyloct-5-en-4-ylcarbamate

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Technology Process of (S,E)-benzyl 8-(tert-butyldiphenylsilyloxy)-2-methyloct-5-en-4-ylcarbamate

There total 5 articles about (S,E)-benzyl 8-(tert-butyldiphenylsilyloxy)-2-methyloct-5-en-4-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1205536-82-8
(S,E)-8-(tert-butyldiphenylsilyloxy)-2-methyloct-5-en-4-amine hydrochloride

: 501-53-1,94274-21-2
benzyl chloroformate

: 1205536-91-9
(S,E)-benzyl 8-(tert-butyldiphenylsilyloxy)-2-methyloct-5-en-4-ylcarbamate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 20 ℃;

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1205536-91-9
(S,E)-benzyl 8-(tert-butyldiphenylsilyloxy)-2-methyloct-5-en-4-ylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1H-imidazole / dichloromethane / 22 h / 20 °C

2.1: Schwartz's reagent / dichloromethane / 0.17 h / 20 °C

2.2: 0.08 h / 0 °C

2.3: 4 h / 20 °C

3.1: triethylamine / tetrahydrofuran / 5 h / 0 - 20 °C

With 1H-imidazole; Schwartz's reagent; triethylamine; In tetrahydrofuran; dichloromethane;

Reference yield:

: 590-86-3
isovaleraldehyde

: 1205536-91-9
(S,E)-benzyl 8-(tert-butyldiphenylsilyloxy)-2-methyloct-5-en-4-ylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: magnesium sulfate; pyridinium p-toluenesulfonate / dichloromethane / 24 h / 25 °C

2.1: Schwartz's reagent / dichloromethane / 0.17 h / 20 °C

2.2: 0.08 h / 0 °C

2.3: 4 h / 20 °C

3.1: triethylamine / tetrahydrofuran / 5 h / 0 - 20 °C

With Schwartz's reagent; pyridinium p-toluenesulfonate; magnesium sulfate; triethylamine; In tetrahydrofuran; dichloromethane;