benzyl (1S)-1-(2-(2-(tert-butyldiphenylsilyloxy)ethyl)cyclopropyl)-3-methylbutylcarbamate

Base Information

Chemical Name:benzyl (1S)-1-(2-(2-(tert-butyldiphenylsilyloxy)ethyl)cyclopropyl)-3-methylbutylcarbamate
CAS No.:1205536-95-3
Molecular Formula:C₃₄H₄₅NO₃Si
Molecular Weight:543.822
Hs Code.:

Synonyms:benzyl (1S)-1-(2-(2-(tert-butyldiphenylsilyloxy)ethyl)cyclopropyl)-3-methylbutylcarbamate

Suppliers and Price of benzyl (1S)-1-(2-(2-(tert-butyldiphenylsilyloxy)ethyl)cyclopropyl)-3-methylbutylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl (1S)-1-(2-(2-(tert-butyldiphenylsilyloxy)ethyl)cyclopropyl)-3-methylbutylcarbamate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of benzyl (1S)-1-(2-(2-(tert-butyldiphenylsilyloxy)ethyl)cyclopropyl)-3-methylbutylcarbamate

There total 6 articles about benzyl (1S)-1-(2-(2-(tert-butyldiphenylsilyloxy)ethyl)cyclopropyl)-3-methylbutylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 75-11-6
diiodomethane

: 1205536-91-9
(S,E)-benzyl 8-(tert-butyldiphenylsilyloxy)-2-methyloct-5-en-4-ylcarbamate

: 1205536-95-3
benzyl (1S)-1-(2-(2-(tert-butyldiphenylsilyloxy)ethyl)cyclopropyl)-3-methylbutylcarbamate

Guidance literature:: diiodomethane; With 1,2-dimethoxyethane; diethylzinc; In dichloromethane; at -20 - 20 ℃; Inert atmosphere;

(S,E)-benzyl 8-(tert-butyldiphenylsilyloxy)-2-methyloct-5-en-4-ylcarbamate; In dichloromethane; at 20 ℃;

Reference yield:

: 1205536-82-8
(S,E)-8-(tert-butyldiphenylsilyloxy)-2-methyloct-5-en-4-amine hydrochloride

: 1205536-95-3
benzyl (1S)-1-(2-(2-(tert-butyldiphenylsilyloxy)ethyl)cyclopropyl)-3-methylbutylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / tetrahydrofuran / 5 h / 0 - 20 °C

2.1: diethylzinc / dichloromethane; 1,2-dimethoxyethane / 0.23 h / -20 - 20 °C / Inert atmosphere

2.2: 10 h / 20 °C

With diethylzinc; triethylamine; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane;

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1205536-95-3
benzyl (1S)-1-(2-(2-(tert-butyldiphenylsilyloxy)ethyl)cyclopropyl)-3-methylbutylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1H-imidazole / dichloromethane / 22 h / 20 °C

2.1: Schwartz's reagent / dichloromethane / 0.17 h / 20 °C

2.2: 0.08 h / 0 °C

2.3: 4 h / 20 °C

3.1: triethylamine / tetrahydrofuran / 5 h / 0 - 20 °C

4.1: diethylzinc / dichloromethane; 1,2-dimethoxyethane / 0.23 h / -20 - 20 °C / Inert atmosphere

4.2: 10 h / 20 °C

With 1H-imidazole; Schwartz's reagent; diethylzinc; triethylamine; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane;