2,3-Diazabicyclo[2.2.1]heptane-2-acetonitrile,3-methyl-(9CI)

Base Information

Chemical Name:2,3-Diazabicyclo[2.2.1]heptane-2-acetonitrile,3-methyl-(9CI)
CAS No.:159583-37-6
Molecular Formula:C₈H₁₃N₃
Molecular Weight:151.211
Hs Code.:
Mol file:159583-37-6.mol

Synonyms:2,3-Diazabicyclo[2.2.1]heptane-2-acetonitrile,3-methyl-(9CI)

Suppliers and Price of 2,3-Diazabicyclo[2.2.1]heptane-2-acetonitrile,3-methyl-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2,3-Diazabicyclo[2.2.1]heptane-2-acetonitrile,3-methyl-(9CI)

Chemical Property:

Boiling Point:136 - 138 °C (24 mmHg)
PSA：30.27000
LogP:0.46928

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,3-Diazabicyclo[2.2.1]heptane-2-acetonitrile,3-methyl-(9CI)

There total 1 articles about 2,3-Diazabicyclo[2.2.1]heptane-2-acetonitrile,3-methyl-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 143-33-9,25596-52-5
sodium cyanide

: 74352-68-4
2-methyl-2,3-diazabicyclo<2.2.1>heptane

: 159583-37-6
1-cyanomethyl-3-methyl-2,3-diazabicyclo<2.2.1>heptane

Guidance literature:: With sodium hydrogensulfite; Yield given. Multistep reaction;
DOI:10.1002/jhet.5570310445

Reference yield: 57.0%

: 159583-37-6
1-cyanomethyl-3-methyl-2,3-diazabicyclo<2.2.1>heptane

: 159583-38-7
1-(2-aminoethyl)-3-methyl-2,3-diazabicyclo<2.2.1>heptane

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; Heating;
DOI:10.1002/jhet.5570310445

Reference yield:

: 159583-37-6
1-cyanomethyl-3-methyl-2,3-diazabicyclo<2.2.1>heptane

: 4-amino-N-<2-(2-methyl-3,6-endomethylenepiperidazino)ethyl>benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 57 percent / lithium aluminum hydride / diethyl ether / Heating

2: 32 percent / pyridine / benzene / 17 h / Ambient temperature

3: 100 percent / H₂ / 5percent Pd/C / ethanol / 1 h / 1810.02 Torr / Ambient temperature

With pyridine; lithium aluminium tetrahydride; hydrogen; palladium on activated charcoal; In diethyl ether; ethanol; benzene;
DOI:10.1002/jhet.5570310445