t-butyl (Z)-1-(benzylcarbamoyl)-2-chlorovinylcarbamate

Base Information

Chemical Name:t-butyl (Z)-1-(benzylcarbamoyl)-2-chlorovinylcarbamate
CAS No.:934169-91-2
Molecular Formula:C₁₅H₁₉ClN₂O₃
Molecular Weight:310.78
Hs Code.:

Synonyms:t-butyl (Z)-1-(benzylcarbamoyl)-2-chlorovinylcarbamate

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Chemical Property of t-butyl (Z)-1-(benzylcarbamoyl)-2-chlorovinylcarbamate

Chemical Property:

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Technology Process of t-butyl (Z)-1-(benzylcarbamoyl)-2-chlorovinylcarbamate

There total 3 articles about t-butyl (Z)-1-(benzylcarbamoyl)-2-chlorovinylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 201938-49-0
t-butyl 1-(benzylcarbamoyl)vinylcarbamate

: 934169-91-2
t-butyl (Z)-1-(benzylcarbamoyl)-2-chlorovinylcarbamate

Guidance literature:: t-butyl 1-(benzylcarbamoyl)vinylcarbamate; With chlorine; In dichloromethane; at -10 ℃; for 0.166667h;

With 1,4-diaza-bicyclo[2.2.2]octane; In acetonitrile; at -10 ℃; for 0.5h; Further stages.;
DOI:10.3987/com-06-10914

Reference yield:

: (R)-tert-butyl 1-(benzylamino)-3-hydroxy-1-oxopropan-2-ylcarbamate

: 934169-91-2
t-butyl (Z)-1-(benzylcarbamoyl)-2-chlorovinylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; methanesulfonyl chloride / CH₂Cl₂ / 0.83 h / 0 - 23 °C

1.2: 20 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / CH₂Cl₂ / 1 h / 20 °C

2.1: chlorine / CH₂Cl₂ / 0.17 h / -10 °C

2.2: 63 percent / 1,4-diazabicyclo[2.2.2]octane / acetonitrile / 0.5 h / -10 °C

With chlorine; methanesulfonyl chloride; triethylamine; In dichloromethane;
DOI:10.3987/com-06-10914

Reference yield:

: 941268-96-8
C₁₆H₂₄N₂O₆S

: 934169-91-2
t-butyl (Z)-1-(benzylcarbamoyl)-2-chlorovinylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 66 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / CH₂Cl₂ / 1.5 h / 23 °C

2.1: chlorine / CH₂Cl₂ / 0.17 h / -10 °C

2.2: 63 percent / 1,4-diazabicyclo[2.2.2]octane / acetonitrile / 0.5 h / -10 °C

With chlorine; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane;
DOI:10.3987/com-06-10914