C₁₆H₁₂Br₂O₃

Base Information

Chemical Name:C₁₆H₁₂Br₂O₃
CAS No.:1400055-34-6
Molecular Formula:C₁₆H₁₂Br₂O₃
Molecular Weight:412.077
Hs Code.:

C<sub>16</sub>H<sub>12</sub>Br<sub>2</sub>O<sub>3</sub>

Synonyms:C₁₆H₁₂Br₂O₃

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Chemical Property of C₁₆H₁₂Br₂O₃

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Technology Process of C₁₆H₁₂Br₂O₃

There total 3 articles about C₁₆H₁₂Br₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1400055-29-9
C₂₁H₂₀Br₂O₅

: 1400055-34-6
C₁₆H₁₂Br₂O₃

Guidance literature:: C₂₁H₂₀Br₂O₅; With 9-O-benzylcupreidine; In toluene; at 23 ℃; for 48h; Reflux;

With toluene-4-sulfonic acid; In toluene; at 80 ℃; for 2h; enantioselective reaction;
DOI:10.1021/ol302273r DOI:10.1021/ol302273r

Reference yield:

: 74003-55-7
3,4-dibromobenzaldehyde

: 1400055-34-6
C₁₆H₁₂Br₂O₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: piperdinium acetate / benzene / 6 h / Reflux

2.1: 9-O-benzylcupreidine / toluene / 48 h / 23 °C / Reflux

2.2: 2 h / 80 °C

With 9-O-benzylcupreidine; piperdinium acetate; In toluene; benzene; 1.1: |Knoevenagel Condensation;
DOI:10.1021/ol302273r DOI:10.1021/ol302273r

Reference yield:

: 1351365-53-1
C₁₄H₁₈O₅

: 1400055-34-6
C₁₆H₁₂Br₂O₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: piperdinium acetate / benzene / 6 h / Reflux

2.1: 9-O-benzylcupreidine / toluene / 48 h / 23 °C / Reflux

2.2: 2 h / 80 °C

With 9-O-benzylcupreidine; piperdinium acetate; In toluene; benzene; 1.1: |Knoevenagel Condensation;
DOI:10.1021/ol302273r DOI:10.1021/ol302273r