(Z)-3-(2-aminoethyl)-5-(4-ethoxybenzylidene)thiazolidine-2,4-dione trifluoroacetate

Base Information

Chemical Name:(Z)-3-(2-aminoethyl)-5-(4-ethoxybenzylidene)thiazolidine-2,4-dione trifluoroacetate
CAS No.:1438408-95-7
Molecular Formula:C₂HF₃O₂*C₁₄H₁₆N₂O₃S
Molecular Weight:406.383
Hs Code.:

Synonyms:(Z)-3-(2-aminoethyl)-5-(4-ethoxybenzylidene)thiazolidine-2,4-dione trifluoroacetate

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Chemical Property of (Z)-3-(2-aminoethyl)-5-(4-ethoxybenzylidene)thiazolidine-2,4-dione trifluoroacetate

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Technology Process of (Z)-3-(2-aminoethyl)-5-(4-ethoxybenzylidene)thiazolidine-2,4-dione trifluoroacetate

There total 3 articles about (Z)-3-(2-aminoethyl)-5-(4-ethoxybenzylidene)thiazolidine-2,4-dione trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1438408-95-7
(Z)-3-(2-aminoethyl)-5-(4-ethoxybenzylidene)thiazolidine-2,4-dione trifluoroacetate

Guidance literature:: With water; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

Reference yield:

: (Z)-5-(4-ethoxybenzylidene)thiazolidine-2,4-dione

: 1438408-95-7
(Z)-3-(2-aminoethyl)-5-(4-ethoxybenzylidene)thiazolidine-2,4-dione trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triphenylphosphine / tetrahydrofuran / 0.08 h / 20 °C

1.2: 45 °C

2.1: dichloromethane / 0.5 h / 20 °C

With triphenylphosphine; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c3ob40199e

Reference yield:

: 10031-82-0
4-ethoxybenzaldehyde

: 1438408-95-7
(Z)-3-(2-aminoethyl)-5-(4-ethoxybenzylidene)thiazolidine-2,4-dione trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: piperidine / ethanol / 24 h / 20 - 75 °C

2.1: triphenylphosphine / tetrahydrofuran / 0.08 h / 20 °C

2.2: 45 °C

3.1: dichloromethane / 0.5 h / 20 °C

With piperidine; triphenylphosphine; In tetrahydrofuran; ethanol; dichloromethane; 1.1: |Knoevenagel Condensation;
DOI:10.1039/c3ob40199e