4,4,5,5-tetramethyl-2-[4-(toluene-2-sulfonyl)-phenyl]-[1,3,2]dioxaborolane

Base Information

Chemical Name:4,4,5,5-tetramethyl-2-[4-(toluene-2-sulfonyl)-phenyl]-[1,3,2]dioxaborolane
CAS No.:1451093-14-3
Molecular Formula:C₁₉H₂₃BO₄S
Molecular Weight:358.266
Hs Code.:

Synonyms:4,4,5,5-tetramethyl-2-[4-(toluene-2-sulfonyl)-phenyl]-[1,3,2]dioxaborolane

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Chemical Property of 4,4,5,5-tetramethyl-2-[4-(toluene-2-sulfonyl)-phenyl]-[1,3,2]dioxaborolane

Chemical Property:

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Technology Process of 4,4,5,5-tetramethyl-2-[4-(toluene-2-sulfonyl)-phenyl]-[1,3,2]dioxaborolane

There total 2 articles about 4,4,5,5-tetramethyl-2-[4-(toluene-2-sulfonyl)-phenyl]-[1,3,2]dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1451093-13-2
1-(chloromethyl)-2-[(4-chlorophenyl)-sulfonyl]benzene

: 73183-34-3
bis(pinacol)diborane

: 1451093-14-3
4,4,5,5-tetramethyl-2-[4-(toluene-2-sulfonyl)-phenyl]-[1,3,2]dioxaborolane

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,4-dioxane; at 102 ℃; for 60h;

Reference yield:

: 13459-60-4
1-(chloromethyl)-2-[(4-chlorophenyl)-sulfanyl]benzene

: 1451093-14-3
4,4,5,5-tetramethyl-2-[4-(toluene-2-sulfonyl)-phenyl]-[1,3,2]dioxaborolane

Guidance literature:: Multi-step reaction with 2 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 15.5 h / -10 - 20 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,4-dioxane / 60 h / 102 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In 1,4-dioxane; dichloromethane;

Reference yield:

: 1227259-08-6
(6-fluoro-3-methyl-4-trifluoromethanesulfonyloxy-naphthalen-2-yl)-acetic acid methyl ester

: 1451093-14-3
4,4,5,5-tetramethyl-2-[4-(toluene-2-sulfonyl)-phenyl]-[1,3,2]dioxaborolane

: 1451093-15-4
{6-fluoro-3-methyl-4-[4-(toluene-2-sulfonyl)-phenyl]-naphthalen-2-yl}-acetic acid methyl ester

Guidance literature:: With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; palladium diacetate; In water; toluene; at 125 ℃; for 15h;