methyl 1-(4-(2-(2-acetamidophenyl)-2-oxoacetamido)benzamido)cyclopentanecarboxylate

Base Information

Chemical Name:methyl 1-(4-(2-(2-acetamidophenyl)-2-oxoacetamido)benzamido)cyclopentanecarboxylate
CAS No.:1622349-81-8
Molecular Formula:C₂₄H₂₅N₃O₆
Molecular Weight:451.479
Hs Code.:

Synonyms:methyl 1-(4-(2-(2-acetamidophenyl)-2-oxoacetamido)benzamido)cyclopentanecarboxylate

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Chemical Property of methyl 1-(4-(2-(2-acetamidophenyl)-2-oxoacetamido)benzamido)cyclopentanecarboxylate

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Technology Process of methyl 1-(4-(2-(2-acetamidophenyl)-2-oxoacetamido)benzamido)cyclopentanecarboxylate

There total 5 articles about methyl 1-(4-(2-(2-acetamidophenyl)-2-oxoacetamido)benzamido)cyclopentanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 702669-44-1
4-(2-(2-acetamidophenyl)-2-oxoacetamido)benzoic acid

: 60421-23-0
cycloleucine methyl ester hydrochloride

: 1622349-81-8
methyl 1-(4-(2-(2-acetamidophenyl)-2-oxoacetamido)benzamido)cyclopentanecarboxylate

Guidance literature:: 4-(2-(2-acetamidophenyl)-2-oxoacetamido)benzoic acid; With ethyl cyanoglyoxylate-2-oxime; diisopropyl-carbodiimide; In N,N-dimethyl-formamide; at 0 ℃; for 0.0833333h;

cycloleucine methyl ester hydrochloride; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 ℃; for 1h;
DOI:10.3390/molecules181214747

Reference yield: 78.0%

: 702669-44-1
4-(2-(2-acetamidophenyl)-2-oxoacetamido)benzoic acid

: 78388-61-1
cycloleucine methyl ester

: 1622349-81-8
methyl 1-(4-(2-(2-acetamidophenyl)-2-oxoacetamido)benzamido)cyclopentanecarboxylate

Guidance literature:: 4-(2-(2-acetamidophenyl)-2-oxoacetamido)benzoic acid; With ethyl cyanoglyoxylate-2-oxime; diisopropyl-carbodiimide; In N,N-dimethyl-formamide; at 0 ℃; for 0.0833333h;

cycloleucine methyl ester; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1016/j.bmcl.2014.11.007

Reference yield:

: 574-17-4
1-acetyl-1H-indole-2,3-dione

: 1622349-81-8
methyl 1-(4-(2-(2-acetamidophenyl)-2-oxoacetamido)benzamido)cyclopentanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: methanol / 0.07 h / 80 °C / 150.01 Torr / Sealed tube

2.1: ethyl cyanoglyoxylate-2-oxime; diisopropyl-carbodiimide / N,N-dimethyl-formamide / 0.08 h / 0 °C

2.2: 1 h / 0 °C

With ethyl cyanoglyoxylate-2-oxime; diisopropyl-carbodiimide; In methanol; N,N-dimethyl-formamide;
DOI:10.3390/molecules181214747