cyclopentyloxy-[4-(pyrrolidine-1-sulfonyl)-phenyl]-acetic acid methyl ester

Base Information

Chemical Name:cyclopentyloxy-[4-(pyrrolidine-1-sulfonyl)-phenyl]-acetic acid methyl ester
CAS No.:1359153-52-8
Molecular Formula:C₁₈H₂₅NO₅S
Molecular Weight:367.466
Hs Code.:

Synonyms:cyclopentyloxy-[4-(pyrrolidine-1-sulfonyl)-phenyl]-acetic acid methyl ester

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Chemical Property of cyclopentyloxy-[4-(pyrrolidine-1-sulfonyl)-phenyl]-acetic acid methyl ester

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Technology Process of cyclopentyloxy-[4-(pyrrolidine-1-sulfonyl)-phenyl]-acetic acid methyl ester

There total 4 articles about cyclopentyloxy-[4-(pyrrolidine-1-sulfonyl)-phenyl]-acetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 91361-92-1
(4-mercapto-phenyl)-acetic acid methyl ester

: 1359153-52-8
cyclopentyloxy-[4-(pyrrolidine-1-sulfonyl)-phenyl]-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: potassium nitrate; chloro-trimethyl-silane / dichloromethane / 24 h / 50 °C / Sealed tube

2: triethylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

3: 4-toluenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 0.5 h / Inert atmosphere

4: dirhodium tetraacetate / dichloromethane / 0.5 h / 25 °C / Inert atmosphere

With chloro-trimethyl-silane; 4-toluenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; potassium nitrate; triethylamine; dirhodium tetraacetate; In dichloromethane; acetonitrile;

Reference yield:

: 53305-12-7
2-(4-(chlorosulfonyl)phenyl)acetic acid methyl ester

: 1359153-52-8
cyclopentyloxy-[4-(pyrrolidine-1-sulfonyl)-phenyl]-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

2: 4-toluenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 0.5 h / Inert atmosphere

3: dirhodium tetraacetate / dichloromethane / 0.5 h / 25 °C / Inert atmosphere

With 4-toluenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; dirhodium tetraacetate; In dichloromethane; acetonitrile;

Reference yield:

: 39161-84-7
4-mercaptophenylacetic acid

: 1359153-52-8
cyclopentyloxy-[4-(pyrrolidine-1-sulfonyl)-phenyl]-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuric acid / 3 h / Reflux

2: potassium nitrate; chloro-trimethyl-silane / dichloromethane / 24 h / 50 °C / Sealed tube

3: triethylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

4: 4-toluenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 0.5 h / Inert atmosphere

5: dirhodium tetraacetate / dichloromethane / 0.5 h / 25 °C / Inert atmosphere

With chloro-trimethyl-silane; 4-toluenesulfonyl azide; sulfuric acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; potassium nitrate; triethylamine; dirhodium tetraacetate; In dichloromethane; acetonitrile;