(4-Methoxy-phenyl)-acetyl azide

Base Information Edit

Chemical Name:(4-Methoxy-phenyl)-acetyl azide
CAS No.:87721-45-7
Molecular Formula:C₉H₉N₃O₂
Molecular Weight:191.189
Hs Code.:
Mol file:87721-45-7.mol

Synonyms:(4-Methoxy-phenyl)-acetyl azide

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Chemical Property of (4-Methoxy-phenyl)-acetyl azide Edit

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Technology Process of (4-Methoxy-phenyl)-acetyl azide

There total 2 articles about (4-Methoxy-phenyl)-acetyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4693-91-8
4-methoxyphenyl-acetic chloride

: 87721-45-7
(4-Methoxy-phenyl)-acetyl azide

Guidance literature:: With sodium azide; In water; acetone; at 0 - 5 ℃; for 0.5h;
DOI:10.1021/jm00099a003

Reference yield:

: 104-01-8
4-Methoxyphenylacetic acid

: 87721-45-7
(4-Methoxy-phenyl)-acetyl azide

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl chloride, dimethylformamide / CH₂Cl₂ / 0.42 h

2: NaN₃ / acetone; H₂O / 0.5 h / 0 - 5 °C

With sodium azide; oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; water; acetone;
DOI:10.1021/jm00099a003