N-cyclohexyl-[4-(2-quinolylmethoxy)phenyl]methoxy-2R,3R-dibenzoyltartarimide

Base Information

Chemical Name:N-cyclohexyl-[4-(2-quinolylmethoxy)phenyl]methoxy-2R,3R-dibenzoyltartarimide
CAS No.:177275-20-6
Molecular Formula:C₄₁H₃₆N₂O₈
Molecular Weight:684.745
Hs Code.:

Synonyms:N-cyclohexyl-[4-(2-quinolylmethoxy)phenyl]methoxy-2R,3R-dibenzoyltartarimide

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Chemical Property of N-cyclohexyl-[4-(2-quinolylmethoxy)phenyl]methoxy-2R,3R-dibenzoyltartarimide

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Technology Process of N-cyclohexyl-[4-(2-quinolylmethoxy)phenyl]methoxy-2R,3R-dibenzoyltartarimide

There total 7 articles about N-cyclohexyl-[4-(2-quinolylmethoxy)phenyl]methoxy-2R,3R-dibenzoyltartarimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 177275-19-3
N-benzyloxy-2R,3R-dibenzoyltartarimide

: 177275-20-6
N-cyclohexyl-[4-(2-quinolylmethoxy)phenyl]methoxy-2R,3R-dibenzoyltartarimide

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / H₂ / 10percent Pd/C / ethyl acetate / 5 h / 760 Torr / Ambient temperature

2: 470 mg / Ph₃P, DEAD / tetrahydrofuran / 4 h / Ambient temperature

With hydrogen; triphenylphosphine; diethylazodicarboxylate; palladium on activated charcoal; In tetrahydrofuran; ethyl acetate;
DOI:10.1016/0957-4166(96)00340-0

Reference yield:

: 64339-95-3
2R,3R-(L)-dibenzoyltartaric acid anhydride

: 177275-20-6
N-cyclohexyl-[4-(2-quinolylmethoxy)phenyl]methoxy-2R,3R-dibenzoyltartarimide

Guidance literature:: Multi-step reaction with 3 steps

1: 2.) SOCl₂ / 1.) THF, RT, 12 h, 2.) CHCl₃, from 0 deg C to RT, 4 h

2: 93 percent / H₂ / 10percent Pd/C / ethyl acetate / 5 h / 760 Torr / Ambient temperature

3: 470 mg / Ph₃P, DEAD / tetrahydrofuran / 4 h / Ambient temperature

With thionyl chloride; hydrogen; triphenylphosphine; diethylazodicarboxylate; palladium on activated charcoal; In tetrahydrofuran; ethyl acetate;
DOI:10.1016/0957-4166(96)00340-0

Reference yield:

: 931-51-1
cyclohexylmagnesiumchloride

: 177275-20-6
N-cyclohexyl-[4-(2-quinolylmethoxy)phenyl]methoxy-2R,3R-dibenzoyltartarimide

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / tetrahydrofuran / 12 h / Ambient temperature

2: 470 mg / Ph₃P, DEAD / tetrahydrofuran / 4 h / Ambient temperature

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran;
DOI:10.1016/0957-4166(96)00340-0