Technology Process of C44H31N4OP
There total 4 articles about C44H31N4OP which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
2-(4-bromophenyl)-1-phenyl-1H-benzimidazole;
With
n-butyllithium;
In
tetrahydrofuran; hexane;
at -78 ℃;
for 1h;
Inert atmosphere;
Schlenk technique;
Dichlorophenylphosphine;
In
tetrahydrofuran; hexane;
at -78 - 20 ℃;
for 12h;
Inert atmosphere;
Schlenk technique;
With
dihydrogen peroxide;
In
dichloromethane; water;
at 20 ℃;
for 1h;
DOI:10.1039/c3tc00801k
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: N,N-dimethyl acetamide / 1 h / 20 °C / Inert atmosphere; Schlenk technique
2.1: acetic acid / 16 h / Inert atmosphere; Reflux; Schlenk technique
3.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere; Schlenk technique
3.2: 12 h / -78 - 20 °C / Inert atmosphere; Schlenk technique
3.3: 1 h / 20 °C
With
n-butyllithium;
In
tetrahydrofuran; hexane; N,N-dimethyl acetamide; acetic acid;
DOI:10.1039/c3tc00801k
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: N,N-dimethyl acetamide / 1 h / 20 °C / Inert atmosphere; Schlenk technique
2.1: acetic acid / 16 h / Inert atmosphere; Reflux; Schlenk technique
3.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere; Schlenk technique
3.2: 12 h / -78 - 20 °C / Inert atmosphere; Schlenk technique
3.3: 1 h / 20 °C
With
n-butyllithium;
In
tetrahydrofuran; hexane; N,N-dimethyl acetamide; acetic acid;
DOI:10.1039/c3tc00801k
