2,2′-(1,4-phenylenebismethyleneoxy)bisbenzeneamine

Base Information

• Chemical Name: 2,2′-(1,4-phenylenebismethyleneoxy)bisbenzeneamine
• CAS No.: 1296756-57-4
• Molecular Formula: C₂₀H₂₀N₂O₂
• Molecular Weight: 320.391
• Mol file: 1296756-57-4.mol

Synonyms:2,2′-(1,4-phenylenebismethyleneoxy)bisbenzeneamine

Chemical Property of 2,2′-(1,4-phenylenebismethyleneoxy)bisbenzeneamine

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,2′-(1,4-phenylenebismethyleneoxy)bisbenzeneamine

There total 6 articles about 2,2′-(1,4-phenylenebismethyleneoxy)bisbenzeneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

C24H24N2O4 (1037911-26-4) → 2,2′-(1,4-phenylenebismethyleneoxy)bisbenzeneamine (1296756-57-4)

Guidance literature:

With sodium hydroxide; In ethanol; water; at 80 ℃;

DOI:10.1002/ejoc.201001312

Reference yield:

C20H16N2O6 (35293-03-9) → 2,2′-(1,4-phenylenebismethyleneoxy)bisbenzeneamine (1296756-57-4)

Guidance literature:

With 5%-palladium/activated carbon; hydrogen; In ethanol; dichloromethane; at 25 ℃; Solvent;

Reference yield:

2-amino-phenol (95-55-6) → 2,2′-(1,4-phenylenebismethyleneoxy)bisbenzeneamine (1296756-57-4)

Guidance literature:

Multi-step reaction with 3 steps

1.1: methanol; water / 5 h / 20 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 80 °C / Inert atmosphere

2.2: 80 °C / Inert atmosphere

3.1: sodium hydroxide / ethanol; water / 80 °C

With potassium carbonate; sodium hydroxide; In methanol; ethanol; water; N,N-dimethyl-formamide;

DOI:10.1002/ejoc.201001312

upstream raw materials:

C₂₄H₂₄N₂O₄

2-amino-phenol

2-(acetylamino)phenol

2-hydroxynitrobenzene

Downstream raw materials:

C₅₆H₄₆N₂O₂P₂