N'-{2,5-dimethyl-4-[(3-phenylisothiazol-5-yl)oxy]phenyl}-N-ethyl-N-methylimidoformamide

Base Information

Chemical Name:N'-{2,5-dimethyl-4-[(3-phenylisothiazol-5-yl)oxy]phenyl}-N-ethyl-N-methylimidoformamide
CAS No.:1239252-55-1
Molecular Formula:C₂₁H₂₃N₃OS
Molecular Weight:365.499
Hs Code.:

Synonyms:N'-{2,5-dimethyl-4-[(3-phenylisothiazol-5-yl)oxy]phenyl}-N-ethyl-N-methylimidoformamide

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Chemical Property of N'-{2,5-dimethyl-4-[(3-phenylisothiazol-5-yl)oxy]phenyl}-N-ethyl-N-methylimidoformamide

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Technology Process of N'-{2,5-dimethyl-4-[(3-phenylisothiazol-5-yl)oxy]phenyl}-N-ethyl-N-methylimidoformamide

There total 3 articles about N'-{2,5-dimethyl-4-[(3-phenylisothiazol-5-yl)oxy]phenyl}-N-ethyl-N-methylimidoformamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 929286-43-1
N-ethyl-N-methylformamide dimethyl acetal

: 1239257-83-0
2,5-dimethyl-4-[(3-phenylisothiazol-5-yl)oxy]aniline

: 1239252-55-1
N'-{2,5-dimethyl-4-[(3-phenylisothiazol-5-yl)oxy]phenyl}-N-ethyl-N-methylimidoformamide

Guidance literature:: In toluene; at 80 ℃;

Reference yield:

: 14208-52-7
5-amino-3-phenylisothiazole

: 1239252-55-1
N'-{2,5-dimethyl-4-[(3-phenylisothiazol-5-yl)oxy]phenyl}-N-ethyl-N-methylimidoformamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: tert.-butylnitrite; copper dichloride / acetonitrile / 60 - 80 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 20 °C

2.2: 3 h / 100 °C

3.1: toluene / 80 °C

With tert.-butylnitrite; sodium hydride; copper dichloride; In N,N-dimethyl-formamide; toluene; acetonitrile; mineral oil;

Reference yield:

: 21905-46-4
5-chloro-3-phenyl-isothiazole

: 1239252-55-1
N'-{2,5-dimethyl-4-[(3-phenylisothiazol-5-yl)oxy]phenyl}-N-ethyl-N-methylimidoformamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 20 °C

1.2: 3 h / 100 °C

2.1: toluene / 80 °C

With sodium hydride; In N,N-dimethyl-formamide; toluene; mineral oil;