2'-[(1Z)-3-[(tetrahydro-2H-pyran-2-yl)oxy]-1-propenyl]cyclohexanecarbothioanilide

Base Information

Chemical Name:2'-[(1Z)-3-[(tetrahydro-2H-pyran-2-yl)oxy]-1-propenyl]cyclohexanecarbothioanilide
CAS No.:224315-10-0
Molecular Formula:C₂₁H₂₉NO₂S
Molecular Weight:359.533
Hs Code.:

Synonyms:2'-[(1Z)-3-[(tetrahydro-2H-pyran-2-yl)oxy]-1-propenyl]cyclohexanecarbothioanilide

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Chemical Property of 2'-[(1Z)-3-[(tetrahydro-2H-pyran-2-yl)oxy]-1-propenyl]cyclohexanecarbothioanilide

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Technology Process of 2'-[(1Z)-3-[(tetrahydro-2H-pyran-2-yl)oxy]-1-propenyl]cyclohexanecarbothioanilide

There total 4 articles about 2'-[(1Z)-3-[(tetrahydro-2H-pyran-2-yl)oxy]-1-propenyl]cyclohexanecarbothioanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 931-51-1
cyclohexylmagnesiumchloride

: 224315-46-2
(Z)-2-((3-(2-isothiocyanatophenyl)allyl)oxy)tetrahydro-2H-pyran

: 224315-10-0
2'-[(1Z)-3-[(tetrahydro-2H-pyran-2-yl)oxy]-1-propenyl]cyclohexanecarbothioanilide

Guidance literature:: In tetrahydrofuran; at 0 - 20 ℃;

Reference yield:

: 110-87-2
3,4-dihydro-2H-pyran

: 224315-10-0
2'-[(1Z)-3-[(tetrahydro-2H-pyran-2-yl)oxy]-1-propenyl]cyclohexanecarbothioanilide

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / camphorsulfonic acid / CH₂Cl₂ / 0.5 h / 20 °C

2: 60 percent / tetrahydrofuran / 0 - 20 °C

With camphor-10-sulfonic acid; In tetrahydrofuran; dichloromethane;

Reference yield:

: 19908-02-2
3-Isothiocyanato-cis-zimtaldehyd

: 224315-10-0
2'-[(1Z)-3-[(tetrahydro-2H-pyran-2-yl)oxy]-1-propenyl]cyclohexanecarbothioanilide

Guidance literature:: Multi-step reaction with 3 steps

1: 7.01 g / NaBH₄ / methanol / -15 °C

2: 100 percent / camphorsulfonic acid / CH₂Cl₂ / 0.5 h / 20 °C

3: 60 percent / tetrahydrofuran / 0 - 20 °C

With sodium tetrahydroborate; camphor-10-sulfonic acid; In tetrahydrofuran; methanol; dichloromethane;