(2R,4S,6S)-4-benzyloxy-6-benzyloxymethyl-2-<(3S,4R)-4-dimethyl-t-butylsiloxy-3,5-dimethylhex-1-ynyl>-2-methoxytetrahydropyran

Base Information

Chemical Name:(2R,4S,6S)-4-benzyloxy-6-benzyloxymethyl-2-<(3S,4R)-4-dimethyl-t-butylsiloxy-3,5-dimethylhex-1-ynyl>-2-methoxytetrahydropyran
CAS No.:116348-90-4
Molecular Formula:C₃₅H₅₂O₅Si
Molecular Weight:580.88
Hs Code.:

Synonyms:(2R,4S,6S)-4-benzyloxy-6-benzyloxymethyl-2-<(3S,4R)-4-dimethyl-t-butylsiloxy-3,5-dimethylhex-1-ynyl>-2-methoxytetrahydropyran

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Chemical Property of (2R,4S,6S)-4-benzyloxy-6-benzyloxymethyl-2-<(3S,4R)-4-dimethyl-t-butylsiloxy-3,5-dimethylhex-1-ynyl>-2-methoxytetrahydropyran

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Technology Process of (2R,4S,6S)-4-benzyloxy-6-benzyloxymethyl-2-<(3S,4R)-4-dimethyl-t-butylsiloxy-3,5-dimethylhex-1-ynyl>-2-methoxytetrahydropyran

There total 1 articles about (2R,4S,6S)-4-benzyloxy-6-benzyloxymethyl-2-<(3S,4R)-4-dimethyl-t-butylsiloxy-3,5-dimethylhex-1-ynyl>-2-methoxytetrahydropyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5460-29-7
2-(3-bromopropyl)isoindole-1,3-dione

: 88096-46-2
(4S,6S)-4-benzyloxy-6-benzyloxymethyltetrahydropyran-2-one

: 97848-39-0
(3R,4S)-2,4-dimethylhex-5-yn-3-yl dimethyl-t-butylsilyl ether

: 116348-90-4
(2R,4S,6S)-4-benzyloxy-6-benzyloxymethyl-2-<(3S,4R)-4-dimethyl-t-butylsiloxy-3,5-dimethylhex-1-ynyl>-2-methoxytetrahydropyran

: 116348-91-5
(2S,4S,6S)-4-benzyloxy-6-benzyloxymethyl-2-<(3S,4R)-4-dimethyl-t-butylsiloxy-3,5-dimethylhex-1-ynyl>-2-methoxytetrahydropyran

Guidance literature:: Yield given. Multistep reaction;

Reference yield: 90.0%

: 116348-90-4
(2R,4S,6S)-4-benzyloxy-6-benzyloxymethyl-2-<(3S,4R)-4-dimethyl-t-butylsiloxy-3,5-dimethylhex-1-ynyl>-2-methoxytetrahydropyran

: 97848-42-5,116348-92-6,116348-93-7
(4S,6S)-4-benzyloxy-6-benzyloxymethyl-2-<(3S,4R)-4-hydroxy-3,5-dimethylhex-1-ynyl>-2-methoxytetrahydropyran

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 8h; Ambient temperature;

Reference yield:

: 116348-90-4
(2R,4S,6S)-4-benzyloxy-6-benzyloxymethyl-2-<(3S,4R)-4-dimethyl-t-butylsiloxy-3,5-dimethylhex-1-ynyl>-2-methoxytetrahydropyran

: 97848-44-7
(2R,3S,6R,8S,10S)-10-benzyloxy-8-benzyloxymethyl-2-isopropyl-3-methyl-1,7-dioxaspiro<5.5>undec-4-ene

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / tetrabutylammonium fluoride / tetrahydrofuran / 8 h / Ambient temperature

2: H₂, quinoline / Lindlar catalyst (5percent Pd-CaCO₃-Pb) / methanol / Ambient temperature

3: CSA / diethyl ether / 0.5 h / Ambient temperature

With quinoline; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; hydrogen; Lindlar catalyst; In tetrahydrofuran; methanol; diethyl ether;