6,6'-diallyl-5,5'-bis(benzyloxy)-1,1',3,3'-tetramethoxy-2,2'-binaphthalene-7,7'-dicarbaldehyde

Base Information

Chemical Name:6,6'-diallyl-5,5'-bis(benzyloxy)-1,1',3,3'-tetramethoxy-2,2'-binaphthalene-7,7'-dicarbaldehyde
CAS No.:950202-15-0
Molecular Formula:C₄₆H₄₂O₈
Molecular Weight:722.835
Hs Code.:

Synonyms:6,6'-diallyl-5,5'-bis(benzyloxy)-1,1',3,3'-tetramethoxy-2,2'-binaphthalene-7,7'-dicarbaldehyde

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Chemical Property of 6,6'-diallyl-5,5'-bis(benzyloxy)-1,1',3,3'-tetramethoxy-2,2'-binaphthalene-7,7'-dicarbaldehyde

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Technology Process of 6,6'-diallyl-5,5'-bis(benzyloxy)-1,1',3,3'-tetramethoxy-2,2'-binaphthalene-7,7'-dicarbaldehyde

There total 6 articles about 6,6'-diallyl-5,5'-bis(benzyloxy)-1,1',3,3'-tetramethoxy-2,2'-binaphthalene-7,7'-dicarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 950202-19-4
[6,6'-diallyl-5,5'-bis(benzyloxy)-7'-hydroxymethyl-1,1',3,3'-tetramethoxy-2,2'-binaphthalenyl-7-yl]methanol

: 950202-15-0
6,6'-diallyl-5,5'-bis(benzyloxy)-1,1',3,3'-tetramethoxy-2,2'-binaphthalene-7,7'-dicarbaldehyde

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 18h;
DOI:10.1039/b707187f

Reference yield:

: 950202-18-3
diethyl 6,6'-diallyl-5,5'-dihydroxy-1,1',3,3'-tetramethoxy-2,2'-binaphthalene-7,7'-dicarboxylate

: 950202-15-0
6,6'-diallyl-5,5'-bis(benzyloxy)-1,1',3,3'-tetramethoxy-2,2'-binaphthalene-7,7'-dicarbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / K₂CO₃; KI / acetone / 18 h / Heating

2: 42 percent / LiAlH₄ / tetrahydrofuran / 18 h / 20 °C

3: 90 percent / pyridinium chlorochromate / CH₂Cl₂ / 18 h / 20 °C

With lithium aluminium tetrahydride; potassium carbonate; pyridinium chlorochromate; potassium iodide; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1039/b707187f

Reference yield:

: 950202-13-8
diethyl 5,5'-bis(allyloxy)-1,1',3,3'-tetramethoxy-2,2'-binaphthalene-7,7'-dicarboxylate

: 950202-15-0
6,6'-diallyl-5,5'-bis(benzyloxy)-1,1',3,3'-tetramethoxy-2,2'-binaphthalene-7,7'-dicarbaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / dimethylformamide / 0.42 h / 170 °C / 12929 Torr / microwave irradiation

2: 90 percent / K₂CO₃; KI / acetone / 18 h / Heating

3: 42 percent / LiAlH₄ / tetrahydrofuran / 18 h / 20 °C

4: 90 percent / pyridinium chlorochromate / CH₂Cl₂ / 18 h / 20 °C

With lithium aluminium tetrahydride; potassium carbonate; pyridinium chlorochromate; potassium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetone; 1: Claisen rearrangement;
DOI:10.1039/b707187f