1-[6,6'-diallyl-5,5'-bis(benzyloxy)-7'-(1-hydroxyethyl)-1,1',3,3'-tetramethoxy-2,2'-binaphthalenyl-7-yl]ethanol

Base Information

• Chemical Name: 1-[6,6'-diallyl-5,5'-bis(benzyloxy)-7'-(1-hydroxyethyl)-1,1',3,3'-tetramethoxy-2,2'-binaphthalenyl-7-yl]ethanol
• CAS No.: 950202-16-1
• Molecular Formula: C₄₈H₅₀O₈
• Molecular Weight: 754.92
• Mol file: 950202-16-1.mol

Synonyms:1-[6,6'-diallyl-5,5'-bis(benzyloxy)-7'-(1-hydroxyethyl)-1,1',3,3'-tetramethoxy-2,2'-binaphthalenyl-7-yl]ethanol

Chemical Property of 1-[6,6'-diallyl-5,5'-bis(benzyloxy)-7'-(1-hydroxyethyl)-1,1',3,3'-tetramethoxy-2,2'-binaphthalenyl-7-yl]ethanol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-[6,6'-diallyl-5,5'-bis(benzyloxy)-7'-(1-hydroxyethyl)-1,1',3,3'-tetramethoxy-2,2'-binaphthalenyl-7-yl]ethanol

There total 1 articles about 1-[6,6'-diallyl-5,5'-bis(benzyloxy)-7'-(1-hydroxyethyl)-1,1',3,3'-tetramethoxy-2,2'-binaphthalenyl-7-yl]ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

6,6'-diallyl-5,5'-bis(benzyloxy)-1,1',3,3'-tetramethoxy-2,2'-binaphthalene-7,7'-dicarbaldehyde (950202-15-0) + methyl iodide (74-88-4) → 1-[6,6'-diallyl-5,5'-bis(benzyloxy)-7'-(1-hydroxyethyl)-1,1',3,3'-tetramethoxy-2,2'-binaphthalenyl-7-yl]ethanol (950202-16-1)

Guidance literature:

methyl iodide; With magnesium; In diethyl ether;

6,6'-diallyl-5,5'-bis(benzyloxy)-1,1',3,3'-tetramethoxy-2,2'-binaphthalene-7,7'-dicarbaldehyde; In tetrahydrofuran; diethyl ether; at 20 ℃; for 18h; Further stages.;

DOI:10.1039/b707187f

Reference yield: 78.0%

1-[6,6'-diallyl-5,5'-bis(benzyloxy)-7'-(1-hydroxyethyl)-1,1',3,3'-tetramethoxy-2,2'-binaphthalenyl-7-yl]ethanol (950202-16-1) → 5,5'-bis(benzyloxy)-7,7',9,9'-tetramethoxy-1,1',3,3'-tetramethyl-1H.1H'-8,8'-bibenzo[g]isochromene

Guidance literature:

With oxygen; palladium dichloride; In water; N,N-dimethyl-formamide; at 20 ℃; for 18h;

DOI:10.1039/b707187f

upstream raw materials:

6,6'-diallyl-5,5'-bis(benzyloxy)-1,1',3,3'-tetramethoxy-2,2'-binaphthalene-7,7'-dicarbaldehyde

methyl iodide