1,2-bis(2-methylphenylimino)acenaphthene

Base Information

Chemical Name:1,2-bis(2-methylphenylimino)acenaphthene
CAS No.:887776-99-0
Molecular Formula:C₂₆H₂₀N₂
Molecular Weight:360.458
Hs Code.:

Synonyms:1,2-bis(2-methylphenylimino)acenaphthene

Suppliers and Price of 1,2-bis(2-methylphenylimino)acenaphthene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,2-bis(2-methylphenylimino)acenaphthene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,2-bis(2-methylphenylimino)acenaphthene

There total 1 articles about 1,2-bis(2-methylphenylimino)acenaphthene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 156398-91-3
{(bis(o-tolylimino)acenaphthene)zinc chloride}

: 887776-99-0
1,2-bis(2-methylphenylimino)acenaphthene

Guidance literature:: With potassium carbonate; In water; Reflux;
DOI:10.1021/om501191c

Reference yield: 86.0%

: 16998-75-7
tetrachlorobis(tetrahydrofurano)molybdenum(IV)

: 887776-99-0
1,2-bis(2-methylphenylimino)acenaphthene

: 884842-82-4
[o-CH₃-C₆H₄-acenaphtene]MoCl₂

Guidance literature:: With Zn; In dichloromethane; (inert Ar atmosphere); 1 equiv. MoCl4(thf)2 added to 3 equiv. diazadieneligand in anhydrous CH2Cl2; zinc added as reducing agent; soln. stirred at room temp for 2 days; supernatant separated by filtration; solvent removed under vacuum; hexane added; crystallization from CH2Cl2/n-hexane at -30 °C;
DOI:10.1016/j.poly.2005.08.027

Reference yield:

: trichlorotritetrahydrofuran chromium(III)

: 887776-99-0
1,2-bis(2-methylphenylimino)acenaphthene

: 943985-45-3
[CrCl₂(C₁₀H₆(CN(o-(CH₃)2C₆H₄))2)]

Guidance literature:: With Zn; In dichloromethane; under inert atm., CrCl3*3THF added to soln. of ligand (1:3) in CH2Cl2, Zn (5 equiv.) added; pptd. (hexane), recrystd. from CH2Cl2/hexane at ambient temp.;
DOI:10.1016/j.inoche.2006.03.011