{(bis(o-tolylimino)acenaphthene)zinc chloride}

Base Information

• Chemical Name: {(bis(o-tolylimino)acenaphthene)zinc chloride}
• CAS No.: 156398-91-3
• Molecular Formula: C₂₆H₂₀Cl₂N₂Zn
• Molecular Weight: 496.754
• Mol file: 156398-91-3.mol

Synonyms:

Chemical Property of {(bis(o-tolylimino)acenaphthene)zinc chloride}

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of {(bis(o-tolylimino)acenaphthene)zinc chloride}

There total 1 articles about {(bis(o-tolylimino)acenaphthene)zinc chloride} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

o-toluidine (95-53-4) + zinc(II) chloride (7646-85-7,24359-56-6) + acenaphthene quinone (82-86-0) → {(bis(o-tolylimino)acenaphthene)zinc chloride} (156398-91-3)

Guidance literature:

the mixture of the starting compds. is stirred at 170°C for 4 h, cooled to 20°C, stirred with diethyl ether; the solid is filtd. off, washed (diethyl ether), air dried;

DOI:10.1002/recl.19941130204

Reference yield:

{(bis(o-tolylimino)acenaphthene)zinc chloride} (156398-91-3) → 1,2-bis(2-methylphenylimino)acenaphthene (887776-99-0)

Guidance literature:

With potassium carbonate; In water; Reflux;

DOI:10.1021/om501191c

upstream raw materials:

o-toluidine

zinc(II) chloride

acenaphthene quinone

Downstream raw materials:

1,2-bis(2-methylphenylimino)acenaphthene