N-(2-hydroxy-propyl)-N-[2-(2,4,6-tribromo-3-methoxy-phenyl)-ethyl]-formamide

Base Information

Chemical Name:N-(2-hydroxy-propyl)-N-[2-(2,4,6-tribromo-3-methoxy-phenyl)-ethyl]-formamide
CAS No.:293756-99-7
Molecular Formula:C₁₃H₁₆Br₃NO₃
Molecular Weight:473.987
Hs Code.:

<i>N</i>-(2-hydroxy-propyl)-<i>N</i>-[2-(2,4,6-tribromo-3-methoxy-phenyl)-ethyl]-formamide

Synonyms:N-(2-hydroxy-propyl)-N-[2-(2,4,6-tribromo-3-methoxy-phenyl)-ethyl]-formamide

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Chemical Property of N-(2-hydroxy-propyl)-N-[2-(2,4,6-tribromo-3-methoxy-phenyl)-ethyl]-formamide

Chemical Property:

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Technology Process of N-(2-hydroxy-propyl)-N-[2-(2,4,6-tribromo-3-methoxy-phenyl)-ethyl]-formamide

There total 6 articles about N-(2-hydroxy-propyl)-N-[2-(2,4,6-tribromo-3-methoxy-phenyl)-ethyl]-formamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 621-37-4
m-hydroxyphenylacetic acid

: 293756-99-7
N-(2-hydroxy-propyl)-N-[2-(2,4,6-tribromo-3-methoxy-phenyl)-ethyl]-formamide

Guidance literature:: Multi-step reaction with 7 steps

1: 61 percent / Et₃N; (EtO)2PO(CN) / tetrahydrofuran / -10 - 20 °C

2: BH₃*THF / tetrahydrofuran / 20 h / Heating

3: 6 h / Heating

4: 3.558 g / 1 h / 75 - 80 °C

5: 96 percent / methanol / 0.5 h / 20 °C

6: 79 percent / 12M HCl / methanol / 2 h / Heating

7: 96 percent / 6 h / Heating

With hydrogenchloride; borane-THF; diethyl cyanophosphonate; triethylamine; In tetrahydrofuran; methanol; 1: Acylation / 2: Reduction / 3: Formylation / 4: Acetylation / 5: Methylation / 6: Hydrolysis / 7: Formylation;
DOI:10.1016/S0968-0896(00)00110-3

Reference yield:

: N-[2-(3-hydroxy-phenyl)-ethyl]-N-(2-hydroxy-propyl)-formamide

: 293756-99-7
N-(2-hydroxy-propyl)-N-[2-(2,4,6-tribromo-3-methoxy-phenyl)-ethyl]-formamide

Guidance literature:: Multi-step reaction with 4 steps

1: 3.558 g / 1 h / 75 - 80 °C

2: 96 percent / methanol / 0.5 h / 20 °C

3: 79 percent / 12M HCl / methanol / 2 h / Heating

4: 96 percent / 6 h / Heating

With hydrogenchloride; In methanol; 1: Acetylation / 2: Methylation / 3: Hydrolysis / 4: Formylation;
DOI:10.1016/S0968-0896(00)00110-3

Reference yield:

: 293756-96-4
3-[2-(2-hydroxy-propylamino)-ethyl]-phenol

: 293756-99-7
N-(2-hydroxy-propyl)-N-[2-(2,4,6-tribromo-3-methoxy-phenyl)-ethyl]-formamide

Guidance literature:: Multi-step reaction with 5 steps

1: 6 h / Heating

2: 3.558 g / 1 h / 75 - 80 °C

3: 96 percent / methanol / 0.5 h / 20 °C

4: 79 percent / 12M HCl / methanol / 2 h / Heating

5: 96 percent / 6 h / Heating

With hydrogenchloride; In methanol; 1: Formylation / 2: Acetylation / 3: Methylation / 4: Hydrolysis / 5: Formylation;
DOI:10.1016/S0968-0896(00)00110-3