3-Cyclohexyl-2-methyl-3-trimethylsilanyloxy-thiopropionic acid S-ethyl ester

Base Information

Chemical Name:3-Cyclohexyl-2-methyl-3-trimethylsilanyloxy-thiopropionic acid S-ethyl ester
CAS No.:130535-74-9
Molecular Formula:C₁₅H₃₀O₂SSi
Molecular Weight:302.553
Hs Code.:

Synonyms:3-Cyclohexyl-2-methyl-3-trimethylsilanyloxy-thiopropionic acid S-ethyl ester

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Chemical Property of 3-Cyclohexyl-2-methyl-3-trimethylsilanyloxy-thiopropionic acid S-ethyl ester

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Technology Process of 3-Cyclohexyl-2-methyl-3-trimethylsilanyloxy-thiopropionic acid S-ethyl ester

There total 2 articles about 3-Cyclohexyl-2-methyl-3-trimethylsilanyloxy-thiopropionic acid S-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 63584-42-9,130535-66-9,63584-50-9
(Z)-1-ethylthio-1-(trimethylsiloxy)propene

: 2043-61-0
cyclohexanecarbaldehyde

: 130535-74-9
3-Cyclohexyl-2-methyl-3-trimethylsilanyloxy-thiopropionic acid S-ethyl ester

Guidance literature:: With (2S)-1-methyl-2-<(N-1-naphthylamino)methyl>pyrrolidine; tin(II) trifluoromethanesulfonate; In various solvent(s); at -78 ℃; for 3h;
DOI:10.1246/cl.1990.1455

Reference yield:

: 63584-42-9,130535-66-9,63584-50-9
(Z)-1-ethylthio-1-(trimethylsiloxy)propene

: 2043-61-0
cyclohexanecarbaldehyde

: 130839-70-2
(2R,3S)-3-Cyclohexyl-2-methyl-3-trimethylsilanyloxy-thiopropionic acid S-ethyl ester

: 127801-80-3
(2S,3R)-3-Cyclohexyl-2-methyl-3-trimethylsilanyloxy-thiopropionic acid S-ethyl ester

: 127801-80-3,130535-74-9,130839-70-2,130839-74-6
(2S,3S)-3-Cyclohexyl-2-methyl-3-trimethylsilanyloxy-thiopropionic acid S-ethyl ester

Guidance literature:: trimethylsilyl trifluoromethanesulfonate; tin(II) oxide; (2S)-1-methyl-2-<(N-1-naphthylamino)methyl>pyrrolidine; In dichloromethane; at -78 ℃; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1246/cl.1990.1147