Ta(η(4)-tribenzylidenemethane)Me2Cl

Base Information

• Chemical Name: Ta(η(4)-tribenzylidenemethane)Me2Cl
• CAS No.: 171508-08-0
• Molecular Formula: C₂₄H₂₄ClTa
• Molecular Weight: 528.855
• Mol file: 171508-08-0.mol

Synonyms:Ta(η(4)-tribenzylidenemethane)Me2Cl

Chemical Property of Ta(η(4)-tribenzylidenemethane)Me2Cl

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Ta(η(4)-tribenzylidenemethane)Me2Cl

There total 2 articles about Ta(η(4)-tribenzylidenemethane)Me2Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

Ta(CH3)3(C6H5)3C4H3 → Ta(η(4)-tribenzylidenemethane)Me2Cl (171508-08-0)

Guidance literature:

In dichloromethane; Irradiation (UV/VIS);

DOI:10.1021/ja00145a044

Reference yield: 99.0%

Ta(CH3)3(C6H5)3C4H3 + zinc(II) chloride (7646-85-7,24359-56-6) → Ta(η(4)-tribenzylidenemethane)Me2Cl (171508-08-0)

Guidance literature:

In tetrahydrofuran; benzene;

DOI:10.1021/ja00145a044

Reference yield: 83.0%

Ta(η(4)-tribenzylidenemethane)Me2Cl (171508-08-0) + lithium diphenylamide (5856-89-3) → (C22H18)Ta(CH3)2(N(C6H5)2)

Guidance literature:

In tetrahydrofuran; stirring (1 h); extracting (toluene), washing (pentane); elem. anal.;

DOI:10.1021/ja981640t

upstream raw materials:

zinc(II) chloride

Downstream raw materials:

Ta(CH₃)2(C₅(CH₃)5)(C₆H₅)3C₄H₃

Ta(CH₃)2(C₅H₅)(C₆H₅)3C₄H₃

(C₁₃H₉)(C₂₂H₁₈)Ta(CH₃)2

(C₅H₄CH₃)(C₂₂H₁₈)Ta(CH₃)2